TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Life Science Applications
Common Drug Screen
Column: DB-5
122-5032
30 m x 0.25 mm, 0.25 µm
Column: DB-17
122-1732
30 m x 0.25 mm, 0.25 µm
Carrier: Hydrogen at 41 cm/sec,
measured at 80°C
Oven: 80°C for 1 min
80-280°C at 10°/min
280°C for 9 min
Injection: Split, 250°C
Split ratio 1:40
Detector: FID, 300°C
DB-5
DB-17
1
3
2
1
4
2
Suggested Supplies
448 www.agilent.com/chem/supplies
9
3
13
25 min
30 min
9
18
6 11
5
10
20
7
16
8 17
14
25
12
22, 24
4
23
19
15
21
20
6 8
5
7
21 23
1617 11 14
13 18
19
10 15
12
22
24
26
25
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper, glass wool, 5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
27
27
26
28
30
29
29 28
31
30, 31
32
32 33
34
33
34
GCLS001
DB-17
Time
DB-5
Time
1. Nicotine 9.87 8.57
2. Phenmetrazine 11.8 9.95
3. Ibuprofen 12.06 10.64
4. Procaine 13.48 14.82
5. Allobarbital 13.91 12.02
6. Aprobarbital 14.14 12.27
7. Butabarbital 14.56 12.76
8. Secobarbital 14.87 14.31
9. Pentobarbital 15.41 13.73
10. Phenacetin 15.72 12.94
11. Amobarbital 15.87 13.43
12. Benzphetamine 16.14 14.96
13. Acetaminophen 16.34 11.12
14. Hydroxyphenamate 16.47 15.31
15. Dimenhydrinate 16.93 13.79
16. Meprobamate 17.12 14.44
17. Benactyzine 17.26 14.71
18. Hexobarbital 17.52 15.22
19. Doxylamine 17.69 15.87
20. Caffeine 18.05 13.11
21. Chlorpheniramine 18.47 16.35
22. Methapyrilene 18.72 16.68
23. Thenyldiamine 18.87 16.85
24. Phenobarbital 19.11 16.29
25. Bromopheniramine 19.71 17.39
26. Chlorcyclizine 20.75 19.13
27. Cocaine 21.32 18.88
28. Pyrrobutamine 22.79 20.89
29. Codeine 24.27 20.66
30. Diazepam 25.27 21.13
31. Morphine 25.36 21.12
32. Hydrocodone 25.98 21.26
33. Oxymorphone 28.27 22.21
34. Heroin 29.32 23.14