TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Life Science Applications
Narcotics
Column: DB-5ms
122-5532
30 m x 0.25 mm, 0.25 µm
Carrier: Helium at 31 cm/sec, measured at 50°C
Oven: 50°C for 0.5 min
50-150°C at 25°/min
150-325°C at 10°/min
Injection: Splitless, 250°C
30 sec purge activation time
Detector: MSD, 300°C transfer line
full scan at m/z 40-380
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Direct connect, single taper,
deactivated, 4 mm ID,
G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-
26s/42/HP, 5181-1267
Narcotics and Adulterants
Column: DB-5
123-5032
30 m x 0.32 mm, 0.25 µm
Carrier: Helium at 40 cm/sec, measured at 140°C
Oven: 140-320°C at 12°/min
320°C for 4 min
Injection: Split, 250°C
Split ratio 1:75
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 0.5 µg/µL each in methanol
456 www.agilent.com/chem/supplies
1
15 16 17
18
Time (min)
19
20 21
1
2
3
2, 3
4
4
5
19 min
6
5
7
6
8
7
1. Dextromethorphan
2. Codeine
3. Dihydrocodeine
4. Norcodeine
5. Ethylmorphine
6. Morphine
7. Normorphine
8. 6-Acetylcodeine
9. 6-Monoacetylmorphine
10. Heroin
8
9
1. Caffeine
2. Ketamine
3. Lidocaine
4. Procaine
5. Cocaine
6. Codeine
7. Morphine
8. 6-Acetylcodeine
9
10
10
9. Diacetylmorphone (Heroin)
10. Quinine
11. Strychnine
11
GCLS017
GCLS016