TABLE OF CONTENTS - BGB Analytik AG

Anticonvulsants
Column: DB-1
125-1032
30 m x 0.53 mm, 1.50 µm
Carrier: Helium at 8 mL/min
Oven: 160°C for 2 min
160-275°C at 15°/min
Injection: Megabore Direct, 250°C
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 100 ng/µL in methanol
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct connect, single taper, deactivated, 4 mm ID, G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
Antihistamines
Column: DB-5
123-5032
30 m x 0.32 mm, 0.25 µm
Carrier: Helium at 40 cm/sec, measured at 55°C
Oven: 55°C for 1 min
55-175°C at 30°/min
175-320°C at 10°/min
320°C for 1 min
Injection: Splitless, 250°C
30 sec purge activation time
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 50 ng/µL each in methanol
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Splitless, single taper,
deactivated, 4 mm ID,
5181-3316
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered,
FN 23-26s/42/HP, 5181-1267
1. Ethosuximide
2. Methsuximide
3. Phensuximide
4. N-Desmethyl methsuximide
5. Phenylethylmalonamide
1 2
www.agilent.com/chem/supplies
1
2, 3
4
5 6
7
8
9
20.5 min
11, 12
10
3
4
10 min
13
Life Science Applications
14
17
16
18
5
15
6
6. Phenobarbital
7. Primidone
8. Carbamazepine
9. Phenytoin
10. 5-Methyl-5-phenylhydantoin
7
8
1. Pheniramine
2. Dimenhydrinate
3. Diphenhydramine
4. Doxylamine
5. Phenyltoloxamine
6. Tripelennamine
7. Methapyrilene
8. Chlorpheniramine
9. Cyclizine
10. Carbinoxamine
11. Diphenylpyraline
12. Bromopheniramine
19
9
20
10
21
GCLS006
13. Thonzylamine
14. Chlorcyclizine
15. Pyrilamine
16. Triprolidine
17. Promethazine
18. Antazoline
19. Clemizole
20. Hydroxyzine
21. Meclizine
22. Cinnanzine
23. Buclizine
22
23
GCLS007
GC and GC/MS
451