TABLE OF CONTENTS - BGB Analytik AG

Blood Pollutants II
Column: DB-ALC1
125-9234
30 m x 0.53 mm, 2.00 µm
Carrier: Helium, 36 cm/sec, measured at 40°C
Oven: 40°C for 5 min
40-210°C at 10°/min
Injection: Split, 250°C
Split ratio 1:10
Detector: FID, 300°C
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct, 1.5 mm ID, 18740-80200
Seal: Gold plated seal, 18740-20885
Residual Solvents, USP 467
Column: DB-624
125-1334
30 m x 0.53 mm, 3.00 µm
Carrier: Helium at 35 cm/sec, measured at 40°C
Oven: 40°C for 20 min
40-90°C at 5°/min
Injection: Megabore Direct, 250°C
5 m phenylmethylsilane deactivated
retention gap
Detector: FID, 300°C
Nitrogen makeup gas at
30 mL/min
2*
4
1*
5*, 12, 13
3*
6
8, 10*
7*, 9
16
1. Methanol*
2. Acetaldehyde*
3. Ethanol*
4. Diethyl ether
5. Isopropyl alcohol*
6. Methylene Chloride
7. Acetone*
8. Acetonitrile
9. Ethyl formate
10. t-Butyl alcohol*
11. 1-Propanol
12. MTBE
13. Hexane
17, 19, 20
11*
14, 21, 24, 15
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22
14. Chloroform
15. sec-Butyl alcohol
16. 2-Chlorobutane
17. MEK (2-Butanone)
18. Ethyl acetate
19. 1,1-Trichloroethane
20. Carbon tetrachloride
21. 1-Chlorobutane
22. Benzene
23. 1-Butanol
24. Heptane
25. Ethylene glycol
26. soamyl alcohol
27. Toluene
23
Life Science Applications
1 2 3 4 5 6 7 8
Time (min)
9 10 11 12 13 14 15
1
2
4
3
5
6
8
7
9
10
13, 14, 15
11
12
16
17
18
19
20
21
30 min
27
1. Methanol
2. Ethanol
3. Ethyl ether
4. Acetone
5. Isopropanol
6. Acetonitrile
7. Methylene chloride
8. tert-Butanol
9. n-Hexane
10. n-Propanol
11. Methyl ethyl ketone (MEK)
12. Ethyl acetate
26
22
25
28. Isopropyl amine (not shown)
29. Ethylbenzene
30. m,p-Xylene
31. o-Xylene
32. DMSO
29
30
28
31
13. Tetrahydrofuran (THF)
14. Chloroform
15. sec-Butanol
16. Cyclohexane
17. Benzene
18. n-Heptane
19. Trichloroethylene
20. n-Butanol
21. 1,4-Dioxane
22. Pyridine
23. Toluene
24. Dimethylformamide (DMF)
23 24
32
GCLS026
GCLS027
GC and GC/MS
461