TABLE OF CONTENTS - BGB Analytik AG

Flavor Mixture
Column: ULTRA 2
19091B-112
25 m x 0.32 mm, 0.52 µm
Carrier: Helium, 90 kPa., 2.2 mL/min constant flow
Oven: 80°C for 1 min
80-210°C at 8°C/min
210°C for 2 min
Injection: Split, 250°C
Split ratio 20:1
Detector: IRD, 280°C
Wide Band MCT, 550 to 4000 cm-1
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper, glass wool, 5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
Chiral Compounds in Essential Oils and Fragrances
Column: HP-Chiral b
19091G-B233
30 m x 0.25 mm, 0.25 µm
Carrier: Hydrogen, 39 cm/sec, Constant pressure
Oven: 65°C for 1 min
65-170° C at 5°C/min
Injection: Split, 250°C
Split ratio 30:1
Detector: FID, 300°C
Sample: 1 µL
0.25 ng/µL each analyte in Hexane
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Split, single taper, low pressure drop, glass wool, 5183-4647
Seal: Gold plated seal, 18740-20885
Syringe: 5 µl tapered, FN 23-26s/42/HP, 5181-1273
Menthol
Column: Cyclodex-b
112-2532
30 m x 0.25 mm, 0.25 µm
Carrier: Hydrogen, 55 cm/sec
Oven: 105°C isothermal
Injection: Split, 250°C
Split ratio 1:100
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 1 µg/µL each chloroform
www.agilent.com/chem/supplies
Foods, Flavors and Fragrance Applications
1. 1,2-Dimethylbenzene
2. Myrcene
3. (-)-Camphene
4. (+)-Camphene
5. (+)-b-Pinene
6. 1S-(-)-b-Pinene
7. Cineole
1. Fenchone
2. Thujone
3. Benzaldehyde
4. trans-Carveol
5. Farnesol
6. cis-Carveol
7. trans-Geraniol
8. Citral
9. Eugenol
10. Vanillin
11. trans-Isoeugenol
12. trans-Citronellyl tiglate
13. cis-Citronellyl tiglate
0
8. (R)-(+)-Citronellal
9. 1S,2R,5S-(+)-Menthol
10. 1R,2S,5R-(-)-Menthol
11. α-Terpineol
12. (+/-)-Isoborneol
13. (+)-Borneol
14. trans-Cinnamaldehyde
1
2
4
3
5
6
7
5 10 15
20
Time (min)
1. (+)-Neomenthol
2. (-)- Neomenthol
3. (+)-Menthol
4. (-)-Menthol
1
2
3
5 10
Time (min)
15
13 min
5
7
4 6
8
8
9
10
11
9 10 13
11
12
1
2
3
14
4
12
GCFF007
GCFF008
GCFF009
GC and GC/MS
401