TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Foods, Flavors and Fragrance Applications
Perfume
Column: HP-INNOWax
19091N-133
30 m x 0.25 mm, 0.25 µm
1. Limonene
2. Linalool
3. Linalyl acetate
4. Benzyl acetate
Carrier:
Oven:
Helium, 30 cm/sec
0.9 mL/min constant flow
80°C for 1 min
80-250°C at 5°C/min
5. Citronellol
6. Benzene ethanol
7. α-Methyl Ionone
250°C for 2 min
8. Carvocrol and geraiol
Injection: Split, 250°C
9. Isoamyl salicylate
Split ratio 20:1
10. n-Amyl salicylate
Detector: MSD, 280°C
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Split, single taper, low pressure drop, glass wool, 5183-4647
Seal: Gold plated seal, 18740-20885
Syringe: 5 µl tapered, FN 23-26s/42/HP, 5181-1273
Lavender Oil Spiked with Camphor
Column: DB-WaxFF
127-7023FF
20 m x 0.10 mm, 0.20 µm
Carrier: H2, 38 psi, 0.33 min, 5 psi/min to 45 psi, hold
Oven: 50°C, 0.33 min
10°C/min to 200°C
200°C hold until last peak elutes
Injection: Split, 250°C
Split ratio 1:650
Detector: FID, 250°C
Column + make-up (N2) in constant flow
Sample: 0.5 µL
Special thanks to Mr. Marin, MANE, France.
9 9.5 10 10.5 11
Time (min)
11.5 12 12.5
400 www.agilent.com/chem/supplies
9.318
9.731
1
11. Commamyl acetate
12. Acetylcedrene
13. Diethyl phthalate
14. Tonalid
15. Coumarin
16. Musk xylene
17. Benzyl benzoate
18. Benzyl salicylate
19. Musk ketone
0
10.530
10.681
1
10.876
2 3
2
5 10 15 20 25 30
Time (min)
11.109
3
11.181
11.27
11.310
4
5
11.461
11.538
6
11.605
7
8
9
11.713
11.876
10
11
12
13
12.214
14
1. Camphor
2. Linalool
15 16
17
3. Linalyl Acetate
12.371
12.508
12.667
18
12.704
19
GCFF006
12.824
12.933
GCFF005
12.965