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GC and GC/MS Petroleum Applications Sulfur Compounds in Natural Gas-Synthetic Mixture Column: HP-1 19091Z-205 50 m x 0.20 mm, 0.50 µm Carrier: Helium Oven: 35°C for 10 min 35-300°C at 7°C/min Injection: Split 100:1 Detector: FPD Sample: 0.5 mL Suggested Supplies Septum: 11 mm Advanced Green septa, 5183-4759 Liner: Direct, 1.5 mm ID, 18740-80200 Seal: Gold plated seal, 18740-20885 Sulfur Compounds in Naphtha Column: HP-PONA 19091S-001 50 m x 0.20 mm, 0.50 µm Carrier: Helium, 26 cm/sec Oven: 35°C for 15 min 35-70°C at 8°C/min 70-130°C at 15°C/min Injection: Split ratio 400:1 Detector: FPD Sample: 3 µL Aromatics Analysis: ASTM D16 Analytes Column: HP-INNOWax 19091N-216 60 m x 0.32 mm, 0.50 µm Carrier: Helium at 20 psi, constant pressure mode Oven: 75°C for 10 min 3°C/min to 100°C 10°C/min to 145°C Injection: Split, 250°C Split ratio 100:1 to 400:1 Detector: FID, 250°C Data aquisition rate at 20 Hz 1 2 3 4 3 4 1 2 5 5 6 7 1 2 3 4 8 42 min 1. Heptane 2. Cyclohexane 3. Octane 4. Nonane 5. Benzene 6. Decane 7. Toluene 8. 1-4-Dioxane 9 101112 13 15 16 18 21 14 19 20 17 22 25 26 24 23 2.5 5.0 7.5 10.0 12.5 Time (min) 15.0 17.5 20.0 22.5 478 www.agilent.com/chem/supplies 6 7 8 9 10 11 12 13 30 min 14 9. Undecane 10. Ethylbenzene 11. p-Xylene 12. m-Xylene 13. Cumene 14. Dodecane 15. o-Xylene 16. Propylebenzene 15 16 1. Hydrogen sulfide 2. Methyl mercaptan 3. Ethyl mercaptan 4. Dimethyl sulfide 5. Isopropyl mercaptan 6. tert-Butyl mercaptan 7. n-Propyl mercaptan 8. Thiophene and sec-Butyl mercaptan 9. Isobutyl mercaptan 10. n-Butyl mercaptan 11. tert-Amyl mercaptan 12. Isoamyl mercaptan 13. n-Amyl mercaptan 14. n-Hexyl mercaptan 15. tert-Dibutyl disulfide 16. n-Octyl mercaptan GCPE023 GCPE022 1. Thiophene 2. Methyl thiophenes 3. Ethyl and dimethyl thiophenes 4. Benzothiophene 17. p-Ethyltoluene 18. m-Ethyltoluene 19. tert-Butylbenzene 20. sec-Butylbenzene 21. Styrene 22. Tridecane 23. Diethylbenzene isomer 24. Diethylbenzene isomer 25. n-Butylbenzene 26. α-Methylstyrene 27. Phenylacetylene 27 GCPE024
Aromatics Analysis - Ethylbenzene Impurities Column: HP-INNOWax 19091N-216 60 m x 0.32 mm, 0.50 µm Carrier: Helium at 20 psi, constant pressure mode Oven: 75°C for 10 min 3°C/min to 100°C 10°C/min to 145°C Injection: Split, 250°C Split ratio 100:1 to 400:1 Detector: FID, 250°C Data aquisition rate at 20 Hz Impurities in p-Xylene - ASTM D3798 Column: HP-INNOWax 19091N-216 60 m x 0.32 mm, 0.50 µm Carrier: Helium, 32 cm/sec, 19.9 psi (60°C), 2.5 mL/min constant flow Oven: 60°C for 1 min 60-92°C at 4°C/min 92°C for 4.5 min 92-220°C at 20°C/min 220°C for 5 min Injection: Split, 220°C Split ratio 100:1 Detector: FID, 270°C Sample: 0.5 µL Neat, 99%+ Ethylene Oxide Synthetic Standard Column: HP-PLOT Q 19095P-QO4 30 m x 0.53 mm, 40.00 µm Carrier: Helium, 25 psi Oven: 50°C for 2 min 50-250°C at 15°C/min Injection: Split ratio 40:1 Detector: FID Sample: 1 µL liquid injection sample 2000 ppm v/v Suggested Supplies Septum: 11 mm Advanced Green septa, 5183-4759 Liner: General Purpose Split/Splitless Liner, taper, glass wool, 5183-4711 Seal: Gold plated seal, 18740-20885 Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267 1 2 3 1 0 2 4 6 8 4 5 2 6 0 5 Time (min) 10 15 3 7 8 9 5.0 7.5 10.0 12.5 15.0 17.5 20.0 Time (min) 1. Non aromatic hydrocarbon 2. Toluene 3. Ethylbenzene 4. p-Xylene 5. m-Xylene 6. o-Xylene 4 5 6 1 2 www.agilent.com/chem/supplies 10 11 Petroleum Applications 12 13 10 12 14 16 Time (min) 14 GCPE025 1. Ethylene oxide 2. 2-Chloropropene 1. Benzene 2. Toluene 3. Undecane 4. Ethylbenzene 5. p-Xylene 6. m-Xylene 7. Isopropylbenzene 8. o-Xylene 9. n-Propylebenzene 10. p-Ethyltoluene 11. m-Ethyltoluene 12. s-Butylbenzene 13. Diethylbenzene 14. Diethylbenzene 3 4 10 11 Time (min) 12 18 20 GCPE028 5 GCPE026 GC and GC/MS 479
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Agilent 1200 Series LC Systems and
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1200 Series Purification Systems De
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Polypropylene Crimp/Snap Top Vials
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Micro-V Vials • Wide opening, 1.5
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8-425 screw top vials 8-425 Screw T
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4 mL screw top vials 4 mL Screw Top
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Certified headspace crimp top vials
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General Purpose Sample and Storage
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Manual crimper and decapper Micro v
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Syringes With a broad selection of
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On-column syringe Push pull Push bu
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CTC Analytics PAL Autosampler Suppl
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X-type fixed needle, G4200-80118 Re
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Sample tray, G6500-80101 Well plate
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Carrier Gas Purification Gas supply
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Triple filter cartridge, 5182-9705
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Reducing union, 0100-0241 Reducing
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Hex Keys, 5064-8211 Screwdrivers De
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Capillary and Megabore ferrule tool
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FID cleaning kit, 9301-0985 GC Budd
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Ink cartridge, 5181-1220 Integrator
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HPIB and GPIB Cables Integrators, I
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Sample Preparation Improve the qual
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Move more quickly toward the method
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R 1 Sulfonic acid-modified divinyl
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O Si O Si (CH2) 17CH3 Si O Si(CH 3)
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Structure of ethyl (C2) silane, cov
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Si O Si O Si OH Structure of diol s
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Additional Agilent SampliQ SPE Phas
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GC and GC/MS For over 40 years, Agi
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BTO septa, 5183-4757 Summary of Pre
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Septa Troubleshooting General Purpo
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MS certified split liner, 5188-6576
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Agilent splitless liners Single tap
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Certified gold inlet seal, 5188-536
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Ferrule Selection Recommendations w
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Universal column nut, 5181-8830 Col
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Glass press-fit connections Quartz
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Capillary Flow Technology Supplies
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A B C Valve Supplies Description Pa
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G1888A Headspace unit G1888A Networ
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1a 5 6 1b 2 3 1c 1d Cool On-Column
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Tips & Tools For new PTV technology
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Flame Ionization Detector (FID) FID
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FID cleaning kit, 9301-0985 Flame I
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Detector fitting Front ferrule Back
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www.agilent.com/chem/supplies Flame
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www.agilent.com/chem/supplies Nitro
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13 14 17 18 1 3 4 5 6 15 16 8 7 Nit
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Sulfur Chemiluminescence Detector (
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Cool On-Column Inlets for Manual In
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7 5890 FID 2 3 4 5 8 9 6 Flame Ioni
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ECD make up gas adapter ECD packed
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GC Standards GC Qualitative Standar
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GC/MS Systems • Less downtime for
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MS interface column nut, 05988-2006
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Electron Impact (EI) Ion Source Ion
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EI high temperature filament, G2590
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Foreline Pump Vacuum Systems and Pu
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MS Test and Performance Samples MS
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Agilent's Über One Test Probe Mixt
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High Efficiency Capillary GC Column
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Spearmint Oil Carrier: A: Helium 25
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Structure of Dimethylpolysiloxane D
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CH 3 CH 3 CH 3 O Si Si O Si CH3 CH3
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CH 3 O Si CH 3 Structure of Dipheny
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CH 3 DB-35ms Chromatograms Environm
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DuraGuard www.agilent.com/chem/supp
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Structure of Dimethylpolysiloxane D
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DB-1 www.agilent.com/chem/supplies
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HP-1 0.32 15 0.25 -60 to 325/350 19
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DB-5 www.agilent.com/chem/supplies
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HP-5 www.agilent.com/chem/supplies
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CH 3 O Si O Si Structure of Dipheny
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O CH 3 C 6H 5 Si O Si CH 3 50% C 6H
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O Si Structure of trifluoropropylme
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DB-1301 • (6%-Cyanopropyl-phenyl)
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-HO H H C C O H H Structure of Poly
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DB-WAX and DB-WaxFF www.agilent.com
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HP-INNOWax Chromatograms Food, Flav
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HP-FFAP Chromatograms Food, Flavors
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Chiral Columns Special Application
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Cyclodex-B Chromatograms Food, Flav
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DB-EVDX Chromatograms Life Sciences
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DB-608 Chromatograms Environmental
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DB-HT SimDis Chromatograms Petroleu
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DB-Dioxin Chromatograms Environment
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HP-VOC • Selectivity engineered f
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Metal Columns DB-ProSteel • Excel
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Custom GC Column Ordering Even thou
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DB-17, 5 in. cage ID (mm) Length (m
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DB-1701P, 5 in. cage ID (mm) Length
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GS-Q, 5 in. cage ID (mm) Length (m)
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HP-20M, 5 in. cage ID (mm) Length (
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HP-PLOT Molesieve, 5 in. cage www.a
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Agilent LTM System CAM LTM Column M
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0.20 12 0.33 -60 to 325/350 128-101
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DB-1ms LTM Column Modules ID (mm) L
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DB-17ms LTM Column Modules ID (mm)
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HP-PLOT Al2O3 "M" LTM Column Module
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HP-PLOT Q LTM Column Modules www.ag
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Fused Silica Tubing Deactivated Tub
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GC Column Application and Method Gu
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Environmental/EPA Methods Analyte T
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ASTM Methods Method Designation Met
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Baseline Instability or Disturbance
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Chlorinated Pesticides, EPA Method
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Organochlorine Pesticides III Colum
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Nitrogen/Phosphorus Containing Pest
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Herbicides II Column: DB-210 122-02
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Environmental Applications, Semivol
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Semivolatile Compounds, EPA Method
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PBDEs by ECD Column: DB-XLB 15 m x
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PCBs by EPA Method 8082 Column: DB-
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Organotin Compounds II Column: HP-5
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EPA Method 8061 (Phthalate Esters)
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Phenols Column: DB-5ms 122-5532 30
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Environmental Applications, Volatil
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Extended Analyte List for EPA Metho
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EPA Method 551 Column: DB-1 122-103
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EPA Air Analysis Method TO-15 (1 pp
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C1 and C2 Halocarbons (Freons) Colu
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Organic Acids Column: DB-FFAP 122-3
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Polyunsaturated Fatty Acid Methyl E
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Free Organic Acids/C4-C5 Isomers Co
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Amines and Nitriles Column: DB-5ms
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Aldehydes and Ketones Column: DB-1
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PFBHA Derivative Column: DB-1 123-1
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HPLC Column Protection Column Prote
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Poroshell 120 • High efficiency a
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Good Peak Shape Over a Wide pH Rang
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Selectivity Changes for Basic Compo
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ZORBAX Eclipse XDB Hardware Descrip
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ZORBAX Eclipse XDB Hardware Descrip
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StableBond SB-C18 Shows Excellent S
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Five Different Bonded Phases Provid
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ZORBAX 80Å StableBond Hardware Des
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Extend-C18 Provides Good Peak Shape
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LiChrospher Reversed-Phase Cartridg
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High Resolution of 24 Amino Acids U
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MicroBore Poroshell 300 Columns Pro
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ZORBAX 300Å StableBond Hardware De
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Novel Bidentate C18-C18 Bonding for
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LC/MS Analysis of Angiotensin on Ex
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ZORBAX GF-250 and GF-450 Gel Filtra
Page 699 and 700:
ZORBAX GF-250 Shows Extended Column
Page 701 and 702:
ZORBAX Bio-SCX Series II Provides M
Page 703 and 704:
High Sensitivity with Capillary Col
Page 705 and 706:
Proteins in a Complex Sample by 2-D
Page 707 and 708:
Multiple Affinity Removal System -
Page 709 and 710:
Column Specifications Multiple Affi
Page 711 and 712:
Multiple Affinity Removal System -
Page 713 and 714:
Tips & Tools The Spin Cartridge Rea
Page 715 and 716:
Luer-Lok syringe, 5188-5250 Luer-Lo
Page 717 and 718:
Protein In-gel Tryptic Digestion Ki
Page 719 and 720:
Peptide Cleanup Pipette Tips Peptid
Page 721 and 722:
HPLC Troubleshooting Symptom Type P
Page 723 and 724:
LC/MS Troubleshooting Symptom Type
Page 725 and 726:
Analgesics: High-Speed PrepHT Isocr
Page 727 and 728:
Cough Formula Mixture: Fast and Eff
Page 729 and 730:
Use ZORBAX Extend-C18 for Alternate
Page 731 and 732:
Peptides: Effect of TFA Concentrati
Page 733 and 734:
Peptide Map - Electronic Flow Contr
Page 735 and 736:
Peptide RP-HPLC/ESI-MS Using NH4OH
Page 737 and 738:
Catecholamines/Biogenic Amines: Rap
Page 739 and 740:
Proteins: Effect of Bonded Phase Co
Page 741 and 742:
BSA Tryptic Digest on RRHT Column:
Page 743 and 744:
Polymethacrylate: GPC Separation Co
Page 745 and 746:
Triton X-114: Decreasing Run-time b
Page 747 and 748:
Organic Acids Separated on ZORBAX S
Page 749 and 750:
Anilines, Separation of Substituted
Page 751 and 752:
Explosives from Soil Extract Column
Page 753 and 754:
Herbicides: Use of Short, Small Par
Page 755 and 756:
Triazine Pesticides on Bonus-RP and
Page 757 and 758:
Plant Hormones: Rapid Gradient Elut
Page 759 and 760:
Aromatic Flavorings Column: Eclipse
Page 761 and 762:
Carbohydrates in Colas Column: ZORB
Page 763 and 764:
Flavoring Agents Column: ZORBAX SB-
Page 765 and 766:
Parabens: High Speed Separation Col
Page 767 and 768:
Water-Soluble Vitamins Column: ZORB
Page 769 and 770:
Fast Vitamin E Analysis on Rapid Re
Page 771 and 772:
Xanthines: Higher Resolution, Same
Page 773 and 774:
Anesthetics, Local: Bonded Phase Se
Page 775 and 776:
Antihistamines Column: ZORBAX Rx-C8
Page 777 and 778:
Chiral Separation of Fluoxetine Ena
Page 779 and 780:
Chiral Separation of Tolperison Ena
Page 781 and 782:
Metronidazole: Updating USP Methods
Page 783 and 784:
Opiate Drugs, Basic Compounds Showi
Page 785 and 786:
Steroids Column A: Eclipse XDB-Phen
Page 787 and 788:
Tricyclic Antidepressants, Screenin
Page 789 and 790:
Dexamethasone, USP Method: Rapid An
Page 791 and 792:
Sulfonamides - Fast Analysis with R
Page 793 and 794:
CE and CE/MS Achieve the sensitivit
Page 795 and 796:
Tips & Tools Agilent offers a varie
Page 797 and 798:
µPAGE Basic Kits Includes 3 µPAGE
Page 799 and 800:
Extended Light Path (Bubble Cell) B
Page 801 and 802:
www.agilent.com/chem/supplies CE an
Page 803 and 804:
www.agilent.com/chem/supplies CE an
Page 805 and 806:
Alignment Interfaces Capillary cass
Page 807 and 808:
CE/MS Accessories www.agilent.com/c
Page 809 and 810:
CE Standards & Reagents Premade buf
Page 811 and 812:
CE System Start-up and Test Kits Ch
Page 813 and 814:
Accessories www.agilent.com/chem/su
Page 815 and 816:
ICP-MS The power you need for ultra
Page 817 and 818:
Gas Line Supplies www.agilent.com/c
Page 819 and 820:
Peristaltic Pump Tubing and Supplie
Page 821 and 822:
Concentric Nebulizer, quartz Use wi
Page 823 and 824:
Quartz spray chamber, G1820-65337 S
Page 825 and 826:
Interface Cone Guide for Agilent IC
Page 827 and 828:
Electron multiplier, 5184-1983 Ion
Page 829 and 830:
Integrated Autosampler Supplies Des
Page 831 and 832:
ISIS Supplies www.agilent.com/chem/
Page 833 and 834:
Miscellaneous Supplies Description
Page 835 and 836:
Single Element Standards Descriptio
Page 837 and 838:
UV-Vis Keeping your system operatin
Page 839 and 840:
Semi-Micro Cell with PTFE Lid Semi-
Page 841 and 842:
Round Aperture Flow Cell Rectangula
Page 843 and 844:
Deuterium lamp assembly, 2140-0605
Page 845 and 846:
UV-Vis Standards & Reagents Our che
Page 847 and 848:
0905-1175..........................
Page 849 and 850:
123-0131LTM........................
Page 851 and 852:
125-5032E..........................
Page 853 and 854:
19091N-133.........................
Page 855 and 856:
200-0185...........................
Page 857 and 858:
5064-8286..........................
Page 859 and 860:
5183-4428..........................
Page 861 and 862:
5982-4411..........................
Page 863 and 864:
840300-908.........................
Page 865 and 866:
959746-906.........................
Page 867 and 868:
G1530-61580........................
Page 869 and 870:
G3270-80026........................
Page 871 and 872:
1,4-Butanediol ....................
Page 873 and 874:
Dicrotophos .......................
Page 875 and 876:
1,2,3,4,6,7,8-Hepta chloro dibenzof
Page 877 and 878:
Octadecane ........................
Page 879 and 880:
Triethylenetetramine (4 isomers) ..
Page 881 and 882:
Caps 8-425 Screw Top No Septa......
Page 883 and 884:
GC Installation Kits Basic Installa
Page 885 and 886:
Moisture Traps Cont. Silica Gel, Gr
Page 887 and 888:
Vials Cont. 2 mL Glass ............
Page 889 and 890:
Easy Ways To Order* • For Interna
Page 891 and 892:
Agilent Technologies Order Form Agi
Page 893 and 894:
Page 895 and 896:
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