TABLE OF CONTENTS - BGB Analytik AG

Phenols I
Column: HP-5ms
19091S-433
30 m x 0.25 mm, 0.25 µm
Carrier: Helium, 33 cm/sec, constant flow
Oven: 35°C for 5 min
35-220°C at 8°C/min
Injection: Splitless, 250°C
Detector: FID, 300°C
Sample: 1 µL
20 µg/mL phenols in methylene chloride
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct connect, single taper, deactivated, 4 mm ID, G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
Phenols II
Column: DB-5ms
122-5536
30 m x 0.25 mm, 0.50 µm
Carrier: Helium at 22 cm/sec,
measured at 100°C
Oven: 100°C for 1 min
100-270°C at 10°/min
Injection: Split, 250°C
Split ratio 1:50
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 50 ng/µL standard
in toluene/p-xylene
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct connect, single taper, deactivated, 4 mm ID, G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
0
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Industrial Chemical Applications
1
2
3
4, 5
1
6
2
1. Phenol
2. 2-Chlorophenol
3. o-Cresol
4. m-Cresol
5. p-Cresol
6. 2,6-Xylenol
7, 8
10
11
2 4 6 8
Time (min)
10 12 14 15
9
13
12
5
3
0 5
10
15
Time (min)
4
6
1. Phenol
2. 2-Chlorophenol
3. 2-Nitrophenol
4. 2,4-Dimethylphenol
5. 2,4-Dichlorophenol
6. 4-Chloro-3-methylphenol
7. 2,4,6-Trinitrophenol
8. 2,4-Dinitrophenol
9. 4-Nitrophenol
10. 2-Methyl-4,6-dinitrophenol
11. Pentachlorophenol
14
7
8
20
9
7. 2,4-Xylenol
8. 2,5-Xylenol
9. 2-Nitrophenol
10. 3,5-Xylenol
11. 2,3-Xylenol
12. 2,4-Dichlorophenol
13. 3,4-Xylenol
14. 2,4,6-Trichlorophenol
15. 2,4-Dinitrophenol
16. 1-Naphthol
15
10
16
GCIC053
11
25
GCIC052
GC and GC/MS
443