TABLE OF CONTENTS - BGB Analytik AG

Hallucinogens
Column: DB-17ms
122-4732
30 m x 0.25 mm, 0.25 µm
Carrier: Helium at 30 cm/sec, measured at 50°C
Oven: 50°C for 0.5 min
50-125°C at 25°/min
125-255°C at 10°/min
255-320°C at 25°/min
320°C for 16 min
Injection:
Splitless, 250°C
30 sec purge activation time
Detector: MSD, 300°C transfer line
full scan at m/z 40-350
Sample: 1 µL of 10-50 ng/µL standard
in methanol
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Direct connect, single taper,
deactivated, 4 mm ID,
G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP,
5181-1267
Sedative Hypnotics
Column: DB-EVDX
128-8522
25 m x 0.20 mm, 0.33 µm
Carrier: Helium at 35 cm/sec, measured at 55°C
Oven: 55°C for 1 min
55-130°C at 25°/min
130-325°C at 15°/min
325°C for 4 min
Injection: Splitless, 250°C
45 sec purge activation time
Detector: MSD, 280°C transfer line
full scan at m/z 35-400
Sample: 1 µL of 50-100 ng/µL standard in methanol
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Direct connect, single taper, deactivated,
4 mm ID, G1544-80730
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP,
5181-1267
1
2
3
6
5
4
7
www.agilent.com/chem/supplies
12
8
9
Life Science Applications
10 12 14 16 18 20 22 24 26 28 30 32 34
Time (min)
1
2
3
4
5
6
7
10
8
1. 4-Methylaminorex
2. Mescaline
3. Dimethyltryptamine
4. Ketimine
5. TCP (Tenocyclidine)
6. PCP
7. Diethyltryptamine
8. Bufotenine
9. Fentanyl
10. Ibogaine
11. LSD
12. Psilocin (peak not shown)
9
10
11
11
1. Ethchlorvynol
2. Ethinamate
3. Pyrithyldione
4. Talbutal
5. Meprobamate
6. Glutethimide
7. Methaqualone
8. Propiomazine
9. Haloperidol
10. Sulpiride
11. Droperidol
GCLS014
3 4 6 8 10 12 14
Time (min)
16 18 20 22
GCLS015
GC and GC/MS
455