TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Life Science Applications
Amphetamines and Precursors - TMS Derivatives
Column: DB-5
121-5023
20 m x 0.18 mm, 0.40 µm
Carrier: Helium at 39 cm/sec, measured at 100°C
Oven: 100-240°C at 10°/min
Injection: Split, 250°C
Split ratio 1:100
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: 1 µL of 2 µg/µL each in pyridine
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper,
glass wool, 5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
Anesthetics
Column: DB-EVDX
128-8522
25 m x 0.20 mm, 0.33 µm
Carrier: Helium at 35 cm/sec, measured at 55°C
Oven: 55°C for 1 min
55-130°C at 25°/min
130-325°C at 15°/min
Injection: Splitless, 250°C
45 sec purge activation time
Detector: MSD, 280°C transfer line
full scan at m/z 35-400
Sample: 1 µL of 50-100 ng/µL standard in methanol
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Splitless, single taper, deactivated, 4 mm ID, 5181-3316
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
1. Phenylacetone
2. Dimethylamphetamine
3. Amphetamine
4. Phentermine
5. Methamphetamine
6. Methyl ephedrine
7. Nicotinamine
8. Ephedrine
450 www.agilent.com/chem/supplies
1
1
2
2
3
4
5
14 min
3
9. Phenacetin
10. 3,4-Methylenedioxyamphetamine (MDA)
11. 3,4-Methylenedioxymethylamphetamine
12. 4-Methyl-2,5-dimethoxyamphetamine (STP)
13. Phenyl ephedrine
14. 3,4-Methylenedioxyethylamphetamine (MDE; Eve)
15. Caffeine
16. Benzphetamine
6 7 8 9
4
5
6
10 11
12
13
1. Salicylamide
2. Benzocaine
3. Lidocaine
4. Procaine
5. Nefopam
6. Mepivacaine
7. Tetracaine
8. Butacaine
9. Dibucaine
7
8
14
16
6 7 8 9 10 11 12 13 14 15
Time (min)
15
GCLS004
9
GCLS005