TABLE OF CONTENTS - BGB Analytik AG

Plant Hormones: Rapid Gradient Elution Separation
Column: ZORBAX Rx/SB-C8
866953-906
4.6 x 75 mm, 3.5 µm
Mobile Phase: A = water with 0.1% TFA
B = Acetonitrile with 0.1% TFA
Flow Rate: 3.0 mL/min
Temperature: 60°C
Detector: UV 245 nm
Sample: Plant hormones
VX Nerve Agent Metabolites by
LC/MS-IS Standard (C13 labeled)
Column: ZORBAX NH2
860700-708
2.1 x 50 mm, 5 µm
Mobile Phase: 1:1 (20 mM Ammonium Actetate
pH 4.5 / Acetonitrile)
Flow Rate: 0.5 ml/min, 1 µl injection
(prepared std in ACN)
Temperature: 350 °C
Detector: ESI-Negative Ion, Gas Flow 12
l/min, Nebulizer 60 psi
Sample: MW
1. Cyclohexyl methylphosphonic
acid 178
2. Pinacolyl methylphosphonic
acid 180
3. Isopropyl methylphosphonic
acid 138
4. Ethyl methylphosphonic acid
124
400000
300000
0
200000
100000
0
200000
0
400000
200000
0
400000
200000
0
TIC
0
www.agilent.com/chem/supplies
1
2
3
1
4 5
6 7
Environmental Applications
8
9
10
2 3
Time (min)
1. Kinetin
2. n-6-Benzyl adenine
3. 3-Indole acetic acid
4. 1-Naphthyl acetamide
5. 3-Indole proprionic acid
6. o-Chlorophenoxy acetic acid
7. p-Chlorophenoxy acetic acid
8. 3-Indole butyric acid
9. 1-Naphthyl acetic acid
10. o-Chlorophenoxy proprionic acid
11. 3,4,5-Trichlorophenoxy acetic acid
12. 3,4,5-Trichlorophenoxy proprionic acid
11
12
4
LCEN022
0 1 2 3 4 5 6 7 8
EIC @128
EIC @140
EIC @183
EIC @185
1
2
2
3 4
0 1 2 3 4 5 6 7 8
Time (min)
1
3
4
LCEN025
LC and LC/MS
757