TABLE OF CONTENTS - BGB Analytik AG

Extended Hydrocarbon Analysis I
Column: GS-Alumina
115-3532
30 m x 0.53 mm
Carrier: Helium at 52 cm/sec (6.7 mL/min),
measured at 100°C
Oven: 100°C for 1 min
100-140°C at 8°/min
140°C for 0.5 min
140-200°C at 30°/min
Injection: Split, 250°C
Split ratio 1:8
Detector: FID, 275°C
Nitrogen makeup gas at 29 mL/min
Sample: 300 µL injection of 100 ppm V
SUMMA cannister mixture
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: Direct, 1.5 mm ID, 18740-80200
Seal: Gold plated seal, 18740-20885
2 4
1
3
5
6
8 10
7
12
9
11 16
13
14
37, 38, 39
32 31 33
36
35
40 34
43, 44, 45
41 42 46
47
25
23 24
15 20 21 22
19
17
18
0 10
20
Time (min)
26, 27, 28
30
29
6 7 8 9
Time (min)
48 49 51 50 52
www.agilent.com/chem/supplies
30
1. Methane
2. Ethane
3. Ethylene
4. Propane
5. Propylene
6. Isobutane
7. Acetylene
8. n-Butane
9. trans-2-Butene
10. 1-Butene
11. cis-2-Butene
12. Cyclopentane
13. Isopentane
14. n-Pentane
15. Propyne
16. 1,3-Butadiene
17. Cyclopentene
18. 3-Methyl-1-butene
19. trans-2-Pentene
20. 2-Methyl-2-butene
21. 1-Pentene
22. cis-2-Pentene
23. Methylcyclopentane
24. 2,2-Dimethylbutane
25. Cyclohexane
26. 2,3-Dimethylbutane
27. 2-Methylpentane
28. 3-Methylpentane
29. Isoprene
GCPE012
Petroleum Applications
30. n-Hexane
31. 4-Methyl-1-pentene
32. trans-2-Hexene
33. 2-Methyl-1-pentene
34. cis-2-Hexene
35. 2,4-Dimethylpentane
36. Methylcyclohexane
37. 2,3-Dimethylpentane
38. 2-Methylhexane
39. 3-Methylhexane
40. n-Heptane
41. Benzene
42. Isooctane (2,2,4-Trimethylpentane)
43. 2,3,4-Trimethylpentane
44. 3-Methylheptane
45. 2-Methylheptane
46. n-Octane
47. Toluene
48. n-Nonane
49. Ethylbenzene
50. m-Xylene
51. p-Xylene
52. o-Xylene
53. Styrene
54. Isopropylbenzene (Cumene)
55. n-Propylbenzene
56. 1,3,5-Trimethylbenzene
57. 1,2,4-Trimethylbenzene
GC and GC/MS
471