TABLE OF CONTENTS - BGB Analytik AG

Halogenated Hydrocarbons II
Column: DB-1
123-1034
30 m x 0.32 mm, 3.00 µm
Carrier: Helium at 35 cm/sec, measured at 35°C
Oven: 35°C for 5 min
35-245°C at 10°/min
245°C for 2 min
Injection: Split, 250°C
Split ratio 1:100
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Sample: In pentane
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper, glass wool, 5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
3, 4
8
5
11
1
2
7, 13, 17
1. 1,1,2-Trichlorotrifluoroethane (Freon-113)
2. 1,1-Dichloroethene
3. Bromoethane (ethyl bromide)
4. Iodomethane
5. 3-Chloropropene (allyl chloride)
6. 1-Chlorobutane
7. 2,2-Dichloropropane
8. trans-1,2-Dichloroethene
9. 1,1,1-Trichloroethane
10. Carbon tetrachloride
11. Methylene chloride
12. Trichloroethene
13. Chloroform
14. Tetrachloroethene
15. 1,2-Dichloropropane
16. 1-Chlorohexane
17. Bromochloromethane
18. 1,1-Dichloroethane
19. 1,2-Dichloroethane
18, 19
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6, 9
10
15, 22
12, 23
27
20
26
24
Industrial Chemical Applications
28
14
16, 25
29
28 min
20
32
33, 34
36
30
20. Iodoform
21. cis-1,3-Dichloropropene
22. Dibromomethane
23. Bromodichloromethane
24. 1,3-Dichloropropane
25. 1,1-Dichloropropane
26. trans-1,3-Dichloropropene
27. 1,1,2-Trichloroethane
28. 1,2-Dibromoethane (EDB)
29. 1,1,1,2-Tetrachloroethane
30. Pentachloroethane
31. Hexachloroethane
32. Bromoform
33. trans-1,4-Dichloro-2-butene
34. 1,2,3-Trichloropropane
35. Hexachlorobutadiene
36. 1,1,2,2-Tetrachloroethane
37. 1,2-Dibromo-3-chloropropane (DBCP)
38. Hexachlorocyclopentadiene
37
31
35
38
GCIC035
GC and GC/MS
435