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TABLE OF CONTENTS - BGB Analytik AG

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LC and LC/MS<br />

GPC-SEC<br />

Polyurethane Resin Quality<br />

Column: ZORBAX SIL PSM 60S<br />

880957-802<br />

6.2 x 250 mm, 5 µm<br />

Mobile Phase: Dimethyl Formamide<br />

Flow Rate: 1.9 mL/min<br />

Temperature: Ambient<br />

Detector: RID<br />

Sample: Polyurethane Resins<br />

Rapid GPC analysis provides measure of performance characteristics<br />

of polyurethane resins.<br />

ZORBAX PSM GPC-SEC Columns<br />

0 1 2<br />

Time (min)<br />

3<br />

672 www.agilent.com/chem/supplies<br />

Agilent ZORBAX PSM Size Exclusion Columns can be used for molecular size separations<br />

on most synthetic and natural polymers. The ZORBAX PSM columns are packed with small<br />

(5 µm) porous silica microspheres (PSM) and are available in two versions. The deactivated<br />

version has been silanized for use with non-polar to relatively polar polymers in nonaqueous or<br />

partially aqueous solvents and is denoted by an S following the column name. The untreated<br />

version is for use with both nonaqueous and aqueous mobile phases. These rigid, siliceous<br />

PSM packings have high mechanical strength and are not swelled or dissolved by any<br />

common organic or aqueous (pH 2-7) mobile phases. For samples of wide molecular weight<br />

distribution, it is useful to couple columns of one or more pore sizes in series, employing<br />

Bimodal Kits. Alternatively, Bimodal columns contain an optimized mixed bed in one column.<br />

ZORBAX PSM GPC-SEC Columns 6.2 mm x 250 mm (5 µm)<br />

Description MW Range Silanized Part No.<br />

PSM 60 5 x 102 - 1 x 104 No 880957-801<br />

PSM 60S 5 x 102 - 1 x 104 Yes 880957-802<br />

PSM 300 3 x 103 - 3 x 105 No 880957-805<br />

PSM 300S 3 x 103 - 3 x 105 Yes 880957-806<br />

PSM 1000 1 x 104 - 1 x 106 No 880957-807<br />

PSM 1000S 1 x 104 - 1 x 106 Yes 880957-808<br />

ZORBAX PSM Bimodal-S 5 x 102 - 1 x 106 Yes 880957-814<br />

PSM Bimodal Kit,<br />

2 columns<br />

5 x 102 - 1 x 104 No 880949-903<br />

Bimodal-S Kit, 2 columns 5 x 102 - 1 x 104 Yes 880949-904<br />

Detector Response<br />

"Good"<br />

"Bad"<br />

LCGPC01

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