TABLE OF CONTENTS - BGB Analytik AG

GC and GC/MS
Industrial Chemical Applications
Halogenated Hydrocarbons I
Column: DB-624
123-1334
30 m x 0.32 mm, 1.80 µm
Carrier: Helium at 35 cm/sec
Oven: 35°C for 5 min
35-245°C at 10°/min
Injection: Split, 250°C
Split ratio 1:50
Detector: FID, 300°C
Nitrogen makeup gas at 30 mL/min
Suggested Supplies
Septum: 11 mm Advanced Green septa, 5183-4759
Liner: General Purpose Split/Splitless Liner, taper, glass wool,
5183-4711
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP, 5181-1267
434 www.agilent.com/chem/supplies
1
2, 3
4
5
6
7
1. Pentane
2. Iodomethane
3. 1,1-Dichloroethene
4. 1,1,2-Trichlorotrifluoroethane (Freon-113)
5. 3-Chloropropene (allyl chloride)
6. Methylene chloride
7. 1,1-Dichloroethane
8. Chloroform
9. 1,1,1-Trichloroethane
10. 1-Chlorobutane
11. Carbon tetrachloride
12. 1,2-Dichloroethane
13. 1,2-Dichloropropane
14. cis-1,2-Dichloropropene
8
9
10
12
11
13
14
15
16
0 5 10 15 20 25
Time (min)
17
18
19
20, 21
15. trans-1,2-Dichloropropene
16. 1,1,2-Trichloroethane
17. 1,1,1,2-Tetrachloroethane
18. 1,2-Dibromoethane (EDB)
19. 1-Chlorohexane
20. trans-1,4-Dichloro-2-butene
21. Iodoform
22. Hexachlorobutadiene
23. 1,2,3-Trichloropropane
24. 1,1,2,2-Tetrachloroethane
25. Pentachloroethane
26. 1,2-Dibromo-3-chloropropane (DBCP)
27. Hexachloroethane
28. Hexachlorocyclopentadiene
22
23
24
25
26
27
28
GCIC034