TABLE OF CONTENTS - BGB Analytik AG

Barbiturates
Column: DB-35ms
122-3832
30 m x 0.25 mm, 0.25 µm
Carrier: Helium at 31 cm/sec, measured at 50°C
Oven: 50°C for 0.5 min
50-150°C at 25°/min
150-300°C at 10°/min
Injection: Splitless, 250°C
30 sec purge activation time
Detector: MSD, 280°C transfer line
full scan at m/z 40-270
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Splitless, single taper,
deactivated, 4 mm ID,
5181-3316
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP,
5181-1267
Benzodiazepines II
Column: DB-35ms
122-3832
30 m x 0.25 mm, 0.25 µm
Carrier: Helium at 31 cm/sec, measured at 50°C
Oven: 50°C for 0.5 min
50-150°C at 25°/min
150-340°C at 10°/min
340°C for 6 min
Injection: Splitless, 250°C
30 sec purge activation time
Detector: MSD, 280°C transfer line
full scan at m/z 40-400
Suggested Supplies
Septum: 11 mm Advanced Green septa,
5183-4759
Liner: Splitless, single taper,
deactivated, 4 mm ID,
5181-3316
Seal: Gold plated seal, 18740-20885
Syringe: 10 µl tapered, FN 23-26s/42/HP,
5181-1267
1
2
2
3
4 6
www.agilent.com/chem/supplies
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13
Life Science Applications
1. Barbital
2. Allobarbital
3. Aprobarbital
4. Butabarbital
5. Butethal
6. Butalbital
7. Amobarbital
8. Talbutal
9. Pentobarbital
11 12 13 14
Time (min)
15 16 17
1
3
4
5
6, 7
8
13
11
14
10
9
12
12
16
14
15
1. Medazepam
2. Halazepam
3. Oxazepam
4. Lorazepam
5. Diazepam
6. Demoxepam
7. Desmethyldiazepam
8. Clobazam
9. Temazepam
15
16
10. Methohexital
11. Secobarbital
12. Hexobarbital
13. Thiopental
14. Cyclopentylbarbital
15. Mephobarbital
16. Thiamylal
17. Phenobarbital
18. Alphenal
19 20 21 22 23 24 25 26 27 28
Time (min)
17
18
10. Flunitrazepam
11. Delorazepam
12. Bromazepam
13. Prazepam
14. Flurazepam
15. Clonazepam
16. Alprazolam
17. Triazolam
17
GCLS010
GCLS011
GC and GC/MS
453