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Scientific Papers Series B Horticulture

Scientific Papers Series B Horticulture

Scientific Papers Series B Horticulture

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Table 1. Sampling procedures applicable for starch industryProduct category Analysis categorySampling procedures applicableInternational standards Legislation (EU / RO) in forceSpecific for quality SR EN ISO 24333:2009 -Contaminants mycotoxins SR EN ISO 24333:2009 Commission Regulation (EC) No 401/2006Food products heavy metals SR EN ISO 24333:2009 Regulation (EC) No 333/2007 pesticides SR EN ISO 24333:2009 Commission Directive 2002/63/ECMicrobiological - Decree ANSVSA 27/2011 non-GMO - 2004/787/EC: Commission RecommendationSpecific for quality SR EN ISO 24333:2009 -Contaminants mycotoxins SR EN ISO 24333:2009 Commission Regulation (EC) No 152/2009 heavy metals SR EN ISO 24333:2009 Commission Regulation (EC) No 152/2009 pesticides SR EN ISO 24333:2009 Commission Directive 2002/63/ECFeed products dioxine SR EN ISO 24333:2009 Commission Directive 2002/70/ECCommission Regulation (EC) No 152/2009; other contaminants SR EN ISO 24333:2009Commission Directive 2002/63/ECMicrobiological - -non-GMO - 2004/787/EC: Commission RecommendationThe analysis categories were split in sixcategories:- specific for quality- mycotoxins- heavy metals- pesticides- microbiological- non-GMOFor each product and analysis category weestablished the specific sampling procedure,taking into account the batch size, theminimum number of elementary samples andquantity of the total sample.For an easier application of this procedure weused an excel file which calculated thesampling frequency depending on the numberof packaging units and pallets.An example for a batch of an approx. 25000kilos is presented in Tables 2 and 3 for foodproducts and in Tables 4 and 5 for feedproducts.The types of analyses performed were groupedin accordance to the sampling proceduresimilarities, so that the analyses specific forquality and those for mycotoxins and heavymetals were presented together (Tables 2 and4), while the analyses for the detection ofpesticides, microbial contamination and thepresence of genetically modified organismswere grouped and included in Tables 3 and 5.In all these tables the abbreviations mean:-parameters measured for all types of samplingprocedures except those involvingmicrobiological analyses:- CP: product code- DA: packed unit weight (kg)- DP: number of packed units in a pallet- DL: batch size (kg)- NP: number of pallets in a batch- NA: number of packed units in a batch- FA: sampling frequency / packed unit- FP: sampling frequency / pallet unit- NPE: number of incremental samples- MPE: size of incremental sample (kg)- PG: size of global sample (kg)- PL: size of laboratory sample (kg)-parameters measured for microbiologicalanalyses:- FP: sampling frequency / pallet unit- NPT: number of tested samples- MPT: tested samples weight-type of food product:- PB: corn- AV: bulk starch- AS: starch packed in 25 kg bags- AB: starch packed in big-bags- GV: bulk glucose syrup417

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