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Handbook of Solvents - George Wypych - ChemTech - Ventech!

Handbook of Solvents - George Wypych - ChemTech - Ventech!

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1558 Denis Kargol<br />

Figure 22.3.4. ASC-200 distillation plant in the explosion-pro<strong>of</strong><br />

room.<br />

Figure 22.3.5. Residue transferred to PE pail.<br />

and thereby promotes evaporation <strong>of</strong> the<br />

solvent. Finally, the solvent vapor reaches<br />

a water-cooler tubular condenser provided<br />

with a cooling water control unit. The condensed,<br />

clean distillate is pumped from<br />

here to the distillate tank. This tank has a<br />

level control and now feeds the clean solvent<br />

directly into the wash plant for a second<br />

wash. The distillation process takes<br />

place fully automatically and lasts about 2<br />

days. Distillation <strong>of</strong> the bottom product takes place independently afterwards. After the residue<br />

has been thickened to a predetermined viscosity, the equipment shuts down automatically.<br />

The still is drained by means <strong>of</strong> a discharge valve at the bottom <strong>of</strong> the cone. The<br />

200-300 kg <strong>of</strong> compact greyish residues are transferred to 20 completely empty 20 liter<br />

plastic pails and then fed to an inexpensive solid waste incineration process. No further<br />

cleaning operations are required at the plant so the stirred distillation unit is ready for use<br />

again immediately.<br />

The plant used at Kabe treats about 200 liters <strong>of</strong> solvent per hour. At about 200 tonnes<br />

per year it is therefore being used to 60-70% <strong>of</strong> its capacity at present. Since its installation,<br />

the distillation plant has been operating for 5 days per week with very little maintenance. A<br />

few mechanics maintain the plant twice a year without external support.

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