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Plenarvorträge - DPG-Tagungen

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Halbleiterphysik Mittwoch<br />

This work was supported by the DFG, SFB 602 TP A7<br />

HL 33.3 Mi 18:45 H14<br />

Annealing of InN layers in a MOVPE reactor investigated by insitu<br />

Spectroscopic Ellipsometry. — •Christoph Werner, Massimo<br />

Drago, Torsten Schmidtling, Udo W. Pohl, and Wolfgang<br />

Richter — TU-Berlin, Institut für Festkörperphysik, Hardenbergstr.<br />

36, 10623 Berlin<br />

Spectroscopic Ellipsometry (SE) is a powerful optical in-situ analysis<br />

tool for growth monitoring of non-cubic materials, as already demonstrated<br />

for GaN epitaxy [1].<br />

Therefore we use SE in order to study annealing of epitaxial InN layers<br />

grown under different gaseous ambients (NH3, N2 and H2) in the growth<br />

temperature regime.<br />

It was found that a hydrogen ambient during annealing leads to a<br />

surface roughening. In contrast, pure nitrogen induces surface smoothening<br />

for temperatures above 540 ◦ C, while roughening becomes dominant<br />

at temperatures exceeding 580 ◦ C. A small addition of ammonia to the<br />

N2 ambient, however, induces surface roughening already at 550 ◦ C. This<br />

shows that, in contrast to GaN, ammonia is not suitable to stabilize InN<br />

at growth temperature. This might be due to the presence of hydrogen<br />

as a consequence of ammonia decomposition.<br />

[1] S. Peters, T. Schmidtling, T. Trepk, U. W. Pohl, J.-T. Zettler, W.<br />

Richter, J. Appl. Phys. 88, 4085 (2000)<br />

HL 33.4 Mi 19:00 H14<br />

MOVPE in-situ monitoring and analysis of substrate deoxidation<br />

of GaSb(100) — •Kristof Möller 1 , Lars Töben 1 , Zadig<br />

Kollonitsch 1 , Christoph Giesen 2 , Michael Heuken 2 , Frank<br />

Willig 1 , and Thomas Hannappel 1 — 1 Hahn-Meitner-Institut, SE-<br />

4, Glienicker Str. 100, D-14109 Berlin, Germany — 2 AIXTRON AG,<br />

Kackertstr. 15-17, D-52072 Aachen, Germany<br />

The crucial deoxidation of GaSb prior to epitaxy was investigated insitu<br />

with reflectance anisotropy spectroscopy (RAS). Substrates were annealed<br />

in an AIX-200 MOVPE reactor in the presence of triethylanti-<br />

HL 34 Hauptvortrag Kouwenhoven<br />

mony in H2 ambient. Deoxidation was carried out between 475 − 575 ◦ C.<br />

RAS signals show the progress in deoxidation for different chemical pretreatments,<br />

annealing temperatures, and annealing times. ”Epi-ready”<br />

substrates annealed without any chemical pre-treatment showed the formation<br />

of anisotropic, nanometer-scaled 3D-structures during deoxidation.<br />

The anisotropic roughness was observed in-situ as an unusual increase<br />

of the RAS signal. This enhanced RAS signal vanished after deoxidation<br />

was completed. RAS Signals showed the absence of roughness<br />

for chemically pre-treated substrates. The surface of the substrates was<br />

investigated with UPS and XPS spectroscopy. The RAS-correlated information<br />

on electronic structure and chemical surface composition is essential<br />

for understanding and improving the deoxidation process of GaSb.<br />

HL 33.5 Mi 19:15 H14<br />

Exzitonenlokalisation in InGaN-Schichten — •T. Finger, J.<br />

Christen, Th. Hempel, A. Dadgar und A. Krost — Institut für<br />

Experimentelle Physik, Otto-von-Guericke Universität Magdeburg<br />

Legierungsunordnung und Entmischung verursachen im ternären In-<br />

GaN mikroskopische Kompositionsfluktuationen, die zu lokalen Potentialfluktuationen<br />

führen. Diese Unordnungseffekte erzeugen ein charakteristisches<br />

Temperaturverhalten der Rekombinationsenergie das von dem<br />

üblichen Eg(T)-Verlauf (z.B. Varshni) signifikant abweicht. Mit sinkender<br />

Temperatur T tritt zunächst eine Rotverschiebung um −σ 2 /kBT auf.<br />

In Folge des Ausfrierens der Ladungsträger bei weiter sinkendem T erfolgt<br />

dann eine Blauverschiebung. Es ergibt sich somit eine charakteristische<br />

s-förmige T-Abhängigkeit der bandkantennahen Lumineszenz. Bei<br />

Erhöhung der Anregungsleistung wird ebenfalls eine Blauverschiebung<br />

beobachtet, die mit einem Auffüllen der statistischen Energieverteilung<br />

erklärt werden kann. Wir haben an 100 nm dicken MOCVD-gewachsenen<br />

InGaN-Epitaxieschichten unterschiedlichen In-Gehaltes (21% - 47%)<br />

Temperatur- und Anregungsdichte-abhängige Lumineszenzmessungen<br />

durchgeführt. Es traten starke Intensitätsmodulationen der Spektren<br />

durch Fabry-Perot Interferenzen in dem Luft+InGaN/GaN (1,2 µm)+Si-<br />

Substrat Schichtpaket auf.<br />

Zeit: Donnerstag 09:30–10:15 Raum: H15<br />

Hauptvortrag HL 34.1 Do 09:30 H15<br />

Spin Qubits with Quantum Dots — •L. P. Kouwenhoven —<br />

Technische Universiteit Delft<br />

Qubits are 2-level systems suitable for control over the level occupation<br />

including superpositions. In solid state, two qubit examples are the effective<br />

2-level system in appropriately designed superconducting devices<br />

and single-electron spin states in semiconductor quantum dots. Qubit<br />

control is demonstrated with NMR-type pulse techniques such as Rabi<br />

flops and spin-echo. The readout of a qubit state is an important part of<br />

the qubit circuit since any backaction can shorten the coherence lifetime.<br />

We discuss a recent realization of a single-shot readout of the spin of a<br />

single electron.<br />

HL 35 Symposium Ferromagnetische Halbleiter<br />

Zeit: Donnerstag 10:15–13:45 Raum: H15<br />

HL 35.1 Do 10:15 H15<br />

Magnetic Anisotropy in Ferromagnetic III-Mn-V Semiconductors:<br />

Issues and Observations — •Jacek K. Furdyna — University<br />

of Notre Dame, Notre Dame, Indiana, USA<br />

Magnetic anisotropy in III-V-based ferromagnetic (FM) semiconductor<br />

alloys (e.g., Ga1−xMnxAs) is interesting from two points of view. First,<br />

it can be “engineered” by imposing appropriate strain conditions on the<br />

FM film; and second, magnetic anisotropy is expected to play an essential<br />

role in designing spin-injection devices based on these materials.<br />

In this paper we present the information on MA in FM semiconductors<br />

obtained through a series of complementary methods: ferromagnetic<br />

resonance (FMR), planar Hall effect, direct imaging of FM domains by<br />

magneto-optical methods, and SQUID magnetization data. Special attention<br />

will be given to the recently-observed re-orientation of the easy<br />

axis in several of the III1−xMnxV alloys as a function of temperature<br />

and/or illumination, and to the somewhat surprising uniaxial anisotropy<br />

in the sample plane which some of these materials exhibit, presumably<br />

as a consequence of surface reconstruction during the growth.<br />

HL 35.2 Do 10:45 H15<br />

Carrier induced ferromagnetism in p type doped II-VI heterostructures<br />

— •David Ferrand — CEA-CNRS-UJF Joint Group,<br />

Laboratoire de Spectrometrie Physique, BP 87 38402 Saint Martin<br />

d’Heres, France<br />

Carrier-induced ferromagnetism in diluted magnetic semiconductors<br />

(D.M.S) has been reported in IV-VI bulk alloys, III-V epilayers and in<br />

II-VI heterostructures. In comparison to III-V, the Curie temperatures<br />

are dramatically lower in II-VI DMS, but II-VI compounds are ideal materials<br />

for fundamental studies, in which localized spins and holes can be<br />

introduced and controlled independently and where dimensionality effects<br />

can be examined in modulation doped heterostructures. We will present<br />

here an overview of our experimental studies, we have done on degenerate<br />

Zn(1−x)MnxTe thick layers and modulation-doped Cd(1−x)MnxTe quantum<br />

wells. Zn(1−x)MnxTe with Mn content up to several percents can be<br />

easily doped p-type using a nitrogen cell up to 10 20 cm −3 , two orders of<br />

magnitude larger than the density for metal-insulator transition. While<br />

the usual antiferromagnetic behavior is observed on the susceptibility of<br />

undoped layers, we observed (SQUID and anomalous Hall effect) positive<br />

Curie-Weiss temperatures between 1.5 and 3K and characteristic ferromagnetic<br />

hysteresis cycles, for layers with hole densities above a few 10 19<br />

cm −3 . In the case of Cd(1−x)MnxTe quantum wells, the magnetic signal

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