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Symposium Organic and Hybrid Systems for Future Electronics Donnerstag or bionic devices require a high degree of functionality as well as a good stability of surfaces against degradation. In this context, the nanopatterning of organically modified surfaces has attracted great attention because such functionalized surfaces offer an excellent passivation and at the same time the possibility to attach different biological species (including DNA, proteins and complex systems). In the present work, strategies for the nanopatterning of chemically modified silicon surfaces using different lithographic approaches will be presented. It will be shown that organic monolayers can be used as a new class of organic-based resists for direct electron-beam writing as well as atomic force microscope nanoscratching. The use of organic monolayers as positive or negative resists will be highlighted by exploiting the contrast in reactivity via chemical deposition (electroless technique) and plating of metals. The high resolution achieved through the use of such organic-based resists will be discussed.The processes presented here open new perspectives for selective deposition and direct patterning of Si surfaces and can be used not only for chemical and electrochemical nanogrowth but also for the nanopatterning of chemical and relevant biological species on semiconductor surfaces. SYOH 5.10 Do 18:00 B Blinking and Emission Quenching of CdSe Nanocrystals in Organic Environments — •Thomas Blaudeck 1 , Abey Issac 2 , Frank Cichos 1 , Edward Zenkevich 3 , Alexander Shulga 3 , and Christian von Borczyskowski 2 — 1 Institut für Physik 123705, TU Chemnitz, 09107 Chemnitz — 2 Institut für Physik 121501, TU Chemnitz, 09107 Chemnitz — 3 Institute of Molecular and Atomic Physics and B.I. Stepanov Institute of Physics National Academy of Sciences, 70 F. Skaryna Avenue, 220072 Minsk, Belarus The interaction of ZnS capped CdSe nanocrystals with their environment is studied on an ensemble and single nanocrystal (NC) level. Individual CdSe NC’s show an emission intermittency (blinking), which is commonly related to an NC photo-ionization by electron tunneling. The statistics of this blinking is found to be independent of the studied NC even though NCs may differ in size and local structure of the surrounding polymer matrix. We analyze the obtained blinking statistics in terms of charge diffusion through trap states in the NCs vicinity and further compare this to current blinking model. Despite the insensitivity of the blinking process to the surrounding polymer matrix a strong interaction between CdSe NCs and pyridyl containing porphyrin molecules is found. The porphyrin molecules self-organize on the NC surface by ligation effects. The interaction of porphyrin and NC introduces a fast non-radiative decay of the NC emission, which is ascribed to an electron transfer process by electron tunneling. The dependence of this tunneling process on the NC size is discussed. SYOH 5.11 Do 18:00 B Temperature-Dependent Growth of Porphyrin and Phthalocyanine Thin Films on Modified Silicon Surfaces — •Christian Kelting 1 , Ossamah Abdallah 2 , Marinus Kunst 2 , Natalia Bazyakina 3 , Dieter Wöhrle 3 , and Derck Schlettwein 1 — 1 Physical Chemistry 1, University of Oldenburg, Germany — 2 Hahn- Meitner- Institute, Berlin, Germany — 3 Institute of Organic and Macromolecular Chemistry, University of Bremen, Germany Films of phthalocyaninatozinc (PcZn) and Tetraphenylporphyrinatozinc (TPPZn) were evaporated on thin films of microcrystalline Si and on hydrogen-terminated Si-wafers (111) as a model surface for microcrystalline Si under conditions of its preparation. The goal is to embed molecular sensitizers into microcrystalline Si as a new concept for thin film solar cells. The maximum substrate temperature for a successful deposition of PcZn and TPPZn was determined to 523 K for PcZn and 423 K for TPPZn on H-Si (111). UV-Vis differential reflection spectroscopy was measured in situ. At 300 K, a 50 nm PcZn film survived for 5h, but slowly evaporated during this time. The morphology of the deposited films was investigated by atomic force microscopy. Larger particles with well- defined shape indicating crystallinity of the films were detected at these higher substrate temperatures. Changes in the crystal structure of PcZn were also observed on the silicon substrates. The alpha- modification of PcZn was found in depositions at 298 K whereas the betamodification was formed at 523 K. SYOH 5.12 Do 18:00 B The influence of carbon on the mono- and multilayer growth of p-quaterphenyl on Au(111) — •Adolf Winkler, Stefan Muellegger, Thomas Haber, and Roland Resel — Solid State Physics, Graz University of Technology The tailoring of the growth mode of ultra-thin organic films is of utmost importance for the application of electronic and optoelectronic devices. As a model system we have studied the monolayer adsorption and the multilayer growth of p-quaterphenyl on clean and carbon covered gold (111) surfaces. TDS, XPS, LEED and XRD-pole figure technique have been applied for these investigations. In TDS, the monolayer peaks are quite different for the Au(111) and Au(111)+C surface. Also LEED shows pronounced differences. The evaluation of the LEED patterns, in combination with quantitative TDS, suggests a monolayer structure with flat lying and side tilted 4P molecules on the clean, but with only side tilted molecules on the C-covered surface. These different monolayer structures lead to different multilayer film structures, as verified by XRD-pole figure technique and XPS. In the former case island growth is preferred, whereas in the latter case layer-like growth dominates. SYOH 5.13 Do 18:00 B Morpholoy and growth of organic semiconductor films on metal surfaces — •S. Söhnchen, S. Lukas, G. Beernink, K. Hänel, A. Birkner, G. Witte, and C. Wöll — Physikalische Chemie I, Ruhr- Universitaet Bochum Organic semiconducting materials have experienced a tremendous amount of attention because of the recent breakthrough in using such materials as active components in electronic or optoelectronic devices. Of particular interest for an optimization of such devices is a detailed understanding of the crystalline structure and growth properties of thin organic semiconductor films deposited on inorganic substrates. In this talk we compare the growth properties observed for pentacene and perylene films grown by OMBE on copper and gold single crystal surfaces as well as on a SAM modified gold surface. Although some of these films are well ordered and partly reveal even an epitaxial growth relation with respect to the substrate [1] they all have a large tendency for dewetting which causes the formation of islands. [1] Lukas et al. Chem. Phys. Chem (in press) SYOH 5.14 Do 18:00 B The Growth of Pentacene on Gold — •F.-J. Meyer zu Heringdorf 1,2 , M.C. Reuter 1 , and R.M. Tromp 1 — 1 IBM T.J. Watson Research Center, Yorktown Heights, USA — 2 present address:Inst. für Laser- und Plasmaphysik, Universität Duisburg-Essen (Campus Essen) We used Low Energy Electron Microscopy and Atomic Force Microscopy to compare the growth of pentacene on Si(111) with the growth of pentacene on Au. In the LEEM Au films are prepared on Si(111) at elevated temperatures and their formation is monitored using quasisimultaneous imaging at different dark field conditions. At low coverages, Au forms a (5 × 2) reconstruction on the Si(111) substrate, and pentacene is observed to grow in the thin film phase, similar to growth on clean silicon. At coverages beyond 3/4 ML of Au, however, a ( √ 3 × √ 3) reconstruction is formed that causes the orientation of the pentacene film to rotate by almost 90 ◦ . The same result is found for pentacene on thick polycrystalline Au films. The adsorption of organic self-assembled monolayers (SAMs) prior to deposition of pentacene has been reported to improve the electrical contact between Au and pentacene. Here we show that thiol based SAMs on Au can restore the growth direction of pentacene to a crystal orientation as seen on Si. This demonstrates that carefully chosen organic substrate termination layers are likely to play a key role in the development of organic thin film semiconductor technology. SYOH 5.15 Do 18:00 B Dislocation Arrangements in Pentacene Films — •Bert Nickel — Ludwig-Maximilians-Universität München Organic molecules are currently at the focus of many research programms due to their applications in molecular electronics. Among the various materials under investigation, pentacene (C22H14), a long, flat, aromatic molecule is particularly promising, in part because pentacene easily forms layered crystals if deposited onto flat, inert surfaces, resulting in highly anisotropic transport properties. We have studied the growth of pentacene films (2-8 monolayers) on modified Si-wafer surfaces by means of synchrotron x-ray diffraction. A quantitative analysis of the
Symposium Organic and Hybrid Systems for Future Electronics Donnerstag Bragg and diffuse scattering allows us to identify screw- and edge dislocations as the main defects on the molecular scale. We quantify dislocation densities obtained for different substrate preparations and discuss their potential relation to transport properties. SYOH 5.16 Do 18:00 B Morphology of Pentacene and Tetraazapentacene grown on SiO2 and vacuum deposited Polytetrafluoroethylene substrates. — •Paul Quinn 1 , S Schrader 1 , L Brehmer 1 , G Jarosz 1 , V Failla 1 , and K Gritsenko 2 — 1 Condensed Matter Physics, Institute of Physics, University of Potsdam, Germany — 2 Institute of Semiconductor Physics NASU, Kiev, Ukraine The growth and morphology of the pentacene based thin films, grown under ultra high vacuum, on SiO2 and vacuum deposited polytetrafluoroethylene was studied using AFM/STM, ellipsometry and polarisation dependent second harmonic generation. The films were grown under a wide range of experimental conditions with variations in the depositions rates, substrate temperatures, and geometries employed to optimise the structural ordering. Polytetrafluoroethylene, of particular interest due to the demand for low-k dielectric materials in semiconductor devices, is shown to form highly ordered films. It was found that the ordering of the pentacene and tetraazapentacene is greatly increased on the polytetrafluoroethylene surface. The ordering of the polytetrafluoroethylene and the ability of this film to promote ordering of the pentacene films is discussed. Acknowledgement: The work was supported by Marie-Curie Host Fellowships: Project MODERN No.HPMD-CT-2001-00083 and by the RTN EUROFET HPRN-CT-2002-00327 SYOH 5.17 Do 18:00 B Substrate and temperature dependent lateral order in N,N’dibutyl-substituted quinacridone monolayer studied by MBD- LEED — •Feng Lin, Dingyong Zhong, Lifeng Chi, and Harald Fuchs — Physikalisches Institut, Universität Münster, D-48149 Münster, Germany Ordered monolayers of N,N’-dibutyl-substituted quinacridone (QA4C) were prepared by vacuum sublimation on Cu(110),Ag(110), and Ag(111) surfaces. Using Low energy electron diffraction that was designed specially to follow the growth processes and thus obtain the kinetics of growth phenomena, the nucleation, grwoth, and superstructures of QA4C monolayers were investigated and compared. The strong interlayer interaction between the QA4C molecules and Cu(110) surface results in very low surface diffusivity at room temperature. Consequently, the commensurate monolayer structure of QA4C was only obtained when annealing the substrate up to 420 K and its crstallographic parameters were determined by the substrate lattice rather than the bulk structure of QA4C itself. While for Ag(110) surface, the QA4C monolayer tended to arrange the molecules in accordance with its bulk crystallography. The microscopic mechanism might be the intralayer interaction of H-bond between molecules which becomes significant since the interlayer interaction is weaker than the case of Cu(110). Temperature induced structural transition was observed on Ag(111), where the six symmetry-equivalent domains at room temperature was changed to a single domain that was more similar to its bulk crystallography at about 200 K. SYOH 5.18 Do 18:00 B Structure and growth morphology of CuPc thin films — •S. Kowarik 1 , A. Gerlach 1 , N. Kishimoto 1,2 , R. Jacobs 1 , and F. Schreiber 1 — 1 Physical and Theoretical Chemistry Laboratory, Oxford University, South Parks Road, Oxford OX1 3QZ, UK — 2 Department of Chemistry, Tohoku University, Aoba-ku, Sendai 980-8578, JAPAN We present a study of the growth and structure of thin films of the organic semiconductor copper-phthalocyanine (CuPc) on SiO2. Films up to a thickness of 2000 ˚A have been studied as a function of the growth parameters (temperature and growth rate) by x-ray diffraction, spectroscopic ellipsometry and atomic force microscopy. The films exhibit a change in morphology from smooth films to needle-shaped crystallites depending on growth temperature. This transition is associated with a change from low crystallinity in smooth films to high crystallinity in rough films. Measurements of the geometric film parameters (thickness and roughness) with spectroscopic ellipsometry and x-ray diffraction allow for a comparison of the two techniques. The results are compared to measurements on thin films of the fluorinated version F16CuPc (1, 2). 1. J. O. Osso et al., Advanced Functional Materials 12, 455-460 (2002). 2. M. I. Alonso et al., Journal of Chemical Physics 119, 6335-6340 (2003). SYOH 5.19 Do 18:00 B Structural and Morphological Properties of N,N´-DiMethyl- 3,4,9,10-PeryleneTetraCarboxylic DiImide Films on Passivated GaAs(100) Substrates — •G. Salvan, S. Silaghi, G. Baumann, T.U. Kampen, R. Scholz, and D.R.T. Zahn — Institut für Physik, Technische Universität Chemnitz, 09107 Chemnitz, Germany Amongst the many-fold applications of organic thin films the use as active interlayers in metal/inorganic semiconductor junctions for the highfrequency and microwave technology is very promising. A route to achieve better device performance is to control the morphology of the organic film by changing the substrate temperature for the film growth. Raman spectroscopy was employed to investigate in situ the structural properties and the morphology of N,N´-DiMethyl-3,4,9,10-PeryleneTetraCarboxylic DiImide films deposited onto S-passivated GaAs(100) substrates in ultrahigh vacuum at various temperatures. Complementary scanning electron microscopy studies revealed that all the films consist of islands. The crystalline nature of these islands was proven by the observation of libronic phonon-like modes of the molecular crystal in the Raman spectra. The decrease in the phonon band widths observed at elevated substrate temperatures is related to an increase in the size of the crystalline domains and improvement of crystallinity. SYOH 5.20 Do 18:00 B Structural investigation of the low temperature order-disorder phase transition of NTCDA on Ag(111) using NIXSW — •C. Stadler, J. Stanzel, M. Scheuermann, S. Hansen, C. Kumpf und E. Umbach — Exp. Physik II, Uni Würzburg The properties of organic thin films largely depend on their interaction with the underlying substrate. For NTCDA on Ag(111) the bonding is regarded as chemisorption as revealed e. g., by photoemission or thermal desorption spectroscopy. Recently an unusual phase transition upon cooling of NTCDA (sub)monolayers on Ag(111) has been observed by electron diffraction studies and other techniques. Upon cooling the long range order disappears below 180 K. Normal Incident X-Ray Standing Waves (NIXSW) measurements were performed using the wiggler beamline ID32 at the ESRF. We report on detailed structural results of different room temperature and low temperature phases, especially on the precise bonding distance between the NTCDA molecules and the Ag substrate. A comparison of the NIXSW results obtained from photoemissionand Auger-yield measurements enables a reasonable correction for nondipolar contributions to the photoeletron yield as well as for electron induced Auger processes. Both effects cannot be neglected for small atomic species. SYOH 5.21 Do 18:00 B Doping and Diffusion Properties of Na in PTCDA Thin Films — •Jens Wüsten, Steffen Berger, Stefan Lach, and Christiane Ziegler — University of Kaiserslautern, Department of Physics, Erwin-Schrödinger-Straße 56, D-67663 Kaiserslautern In order to investigate the electronic and vibronic properties of n-doped PTCDA (perylene-3,4,9,10-tetracarboxylic-dianhydride), thin films were grown under UHV conditions. The n-doping was performed by subsequently evaporating sodium (Na) from a dispenser source, followed by one or several annealing steps to reach a homogeneous distribution of the dopant throughout the layer. Experimental results from electronic (XPS/UPS/IPE), conductivity, Seebeck, vibration (FT-IR), angle resolved XPS and SIMS measurements of Na doped PTCDA before and after annealing will be presented. The changes in the elctronic structure and the electrical properties show that doping is already established after Na evaporation. However, the results suggest that the model of an initially built doped surface layer and a subsequent diffusion of Na into the PTCDA bulk during the annealing step is incorrect. In fact evidences could be found, that the deposited dopant initially establishes a homogeneous distribution in the PTCDA layer and is partially removed during the annealing step. SYOH 5.22 Do 18:00 B Radiotracer diffusion measurements of noble metal atoms in crystalline organic films — •Michael Scharnberg 1 , Jörn Kanzow 1 , Rainer Adelung 1 , Klaus Rätzke 1 , Franz Faupel 1 , Christoph Pannemann 2 , Ulrich Hilleringmann 2 , and Jens Pflaum 3 — 1 Technische Fakultät, CAU Kiel, Kaiserstr. 2, 24143 Kiel — 2 Department EIM-E/Sensorik, Univ. Paderborn — 3 3. Physikalisches Institut, Univ. Stuttgart The application of organic field effect transistors (OFETs) for large
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Arbeitskreis Biologische Physik Fre
Page 441 and 442: Arbeitskreis Biologische Physik Fre
Page 459 and 460: Arbeitskreis Physik sozio-ökonomis
Page 467 and 468: Symposium Fat-Tail Distributions -
Page 469 and 470: Symposium Life Sciences on the Nano
Page 483 and 484: Symposium Non-Fermi Liquids in Quan
Page 485 and 486: Symposium Functional Nanoparticles
Page 487 and 488: Symposium Organic and Hybrid System
Page 491: Symposium Organic and Hybrid System
Page 507 and 508: Symposium Physics of Foams Mittwoch
Page 509 and 510: Symposium Physics of Foams Mittwoch
Page 511 and 512: Symposium Quantum Shot Noise in Nan
Page 513 and 514: Symposium X-RAY Magneto-Optics Tage
Page 515 and 516: Symposium X-RAY Magneto-Optics Dien
Page 517 and 518: Lehrertage Regensburg Hauptvorträg
Page 519 and 520: A. D., Mirlin .................HL 1
Page 521 and 522: Breidenbach, Boris ........ AKB 50.
Page 523 and 524: Elli, Alexandra .............SYLS 3
Page 525 and 526: Greer, Lindsay ......... M 9.1, M 1
Page 527 and 528: Horn-von Hoegen, M. O 13.2, O 14.40
Page 529 and 530: Korn, Tobias ...............MA 13.6
Page 531 and 532: Martin, Tobias ............. MA 13.
Page 533 and 534: Partyka, Ewa ................ M 18.
Page 535 and 536: Rugeramigabo, Eddy Patrick O 14.38,
Page 537 and 538: Sihler, J. .................... DS
Page 539 and 540: Volz, K. .................... HL 44
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