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Tiefe Temperaturen Montag<br />

vated by its proximity to a quantum phase transition, the isoelectronic<br />

compound YbIr2Si2 has not yet been investigated. We have synthesized<br />

polycrystalline and single crystalline samples of YbIr2Si2 and investigated<br />

their physical properties. Depending on synthesis conditions the<br />

samples take either body-centred (ThCr2Si2 structure- I-type) or primitive<br />

tetragonal (CaBe2Ge2 structure- P-type) structure. P-type sample<br />

shows AF order below 700 mK. I-type sample does not show any signature<br />

of magnetic order down to 100 mK. The magnetic susceptibility for<br />

this sample is highly anisotropic with effective moment close to that expected<br />

for Yb 3+ ions. The resistivity is nearly temperature independent<br />

at high temperature followed by a rapid decrease below 100 K similar to<br />

Kondo lattice/heavy fermion system. The resistivity does not show any<br />

anomaly due to either magnetic or superconducting transition down to<br />

20 mK. Further, the resistivity at low temperature follows ρ(T) = ρ0 +<br />

AT n with n =1.3 instead of n = 2 expected from Fermi Liquid theory.<br />

The specific heat is also Non-Fermi-Liquid (NFL) type as C/T continues<br />

to increase with decreasing T down to 350 mK where C/T = 0.6 J/(mol<br />

K 2 ). Thus, I-type YbIr2Si2 is a new heavy fermion compound situated<br />

close to the quantum critical point and exhibits NFL behaviour.<br />

TT 7.8 Mo 16:30 H19<br />

Investigation of the magnetic and the superconducting states of<br />

CeCu2Si2 using large single crystal. — •H.S. Jeevan 1 , M. Deppe 1 ,<br />

O. Stockert 1 , R. Borth 1 , E. Faulhaber 2 , C. Geibel 1 , and F.<br />

Steglich 1 — 1 Max Planck Institute for Chemical Physics of Solids,<br />

Dresden — 2 TU Dresden, IAPD, D-01062 Dresden, Germany.<br />

The discovery of superconductivity in CeCu2Si2 in 1979 opened the<br />

field of unconventional superconductivity in strongly correlated systems.<br />

Later on, another unconventional phase, the A-phase, of presumably<br />

magnetic character was found to compete with the superconducting phase<br />

in CeCu2Si2. Despite more than 20 years of intensive research, the nature<br />

of the superconducting phase and of the A-phase as well as the interac-<br />

TT 8 Postersitzung I: Supraleitung<br />

tion between both are very far from being understood. A major problem<br />

is the lack of large single crystals with well defined physical properties.<br />

This prevents e.g. a study of the magnetic structure and magnetic excitations<br />

of this compound with neutron scattering, which would allow<br />

a much deeper insight into the nature of these unconventional phases.<br />

We have developed a self-flux growth method, which allows the growth<br />

of large CeCu2Si2 single crystal with well defined properties. The ground<br />

state can be tuned by changing growth parameters. We have investigated<br />

the magnetic and the superconducting ground state using specific<br />

heat, resistivity and susceptibility measurements. The preliminary neutron<br />

scattering measurements allow us to determine for the first time<br />

the magnetic structure of the A-phase. We shall analyse and discuss the<br />

physical properties of these single crystals and their relation to growth<br />

parameters.<br />

TT 7.9 Mo 16:45 H19<br />

Weak itinerant metamagnetism at the quantum phase transition<br />

of ZrZn2 — •M. Uhlarz 1 , C. Pfleiderer 1 , and S. M. Hayden<br />

2 — 1 Physikalisches Institut, Universität Karlsruhe, D-76128 Karlsuhe,<br />

Germany — 2 H. H. Wills Physics Laboratory, University of Bristol,<br />

Bristol, BS8 1TL, UK<br />

It is generally assumed that the coexistence of band-ferromagnetism<br />

with superconductivity, recently discovered in ZrZn2 [1], is connected<br />

with the proximity of ZrZn2 to a quantum critical point. We have revisited<br />

the question of quantum criticality in ZrZn2 in a detailed study of<br />

the pressure dependence of the magnetisation of single crystals of ZrZn2<br />

up to 21kbar at temperatures down to 1.5K and magnetic field up to<br />

12T. In the vicinity of the critical pressure we observe evidence for weak<br />

first order behaviour and itinerant metamagnetism. The evolution of the<br />

magnetic state in ZrZn2 is compared with that observed in the superconducting<br />

ferromagnets UGe2 and URhGe.<br />

[1] C. Pfleiderer et al., Nature 412 (2001) 58.<br />

Zeit: Montag 14:30–19:00 Raum: Poster A<br />

TT 8.1 Mo 14:30 Poster A<br />

In-situ deposition of MgB2 thin films by magnetron sputtering<br />

and thermal evaporation — •R. Schneider, A.G. Zaitsev, J.<br />

Geerk, G. Linker, and F. Ratzel — Forschungszentrum Karlsruhe,<br />

Institut für Festkörperphysik<br />

We report on two approaches to the in-situ synthesis of superconducting<br />

MgB2 thin films. In the first approach, Mg and B were simultaneously<br />

sputtered from two separate planar targets. The substrate temperature<br />

Ts was limited to a small range of 290 to 320 ◦ C. The resulting films on<br />

sapphire substrates were c-axis textured with low growth quality. Their<br />

transition temperature Tc reached a maximum of 24 K with a transition<br />

width of 0.6 K. A short-time in-situ annealing at 600 ◦ C improved Tc to<br />

28 K. In the second approach, the Mg sputter source was replaced by<br />

a specially designed Mg evaporator. Due to this intense Mg source Ts<br />

could be increased to 440 ◦ C, and Tc of the ”as-grown” films rose to 33<br />

K. Short-time in-situ annealing after the film deposition enhanced Tc to<br />

36 K. For these films we also measured a high critical current density of<br />

15 MA/cm 2 at 6 K.<br />

TT 8.2 Mo 14:30 Poster A<br />

Preparation, Structure, and Properties of Hg,Re-Containing<br />

High-Temperature Superconductor Thin Films — •Abouelwafa<br />

Salem, Gerhard Jakob und Hermann Adrian — Institut für Physik,<br />

Johannes Gutenberg–Universität, 55099<br />

Fully textured (Hg0.9Re0.1)Ba2CaCu2O6+δ (HgRe-1212) thin films have<br />

been prepared by pulsed laser deposition (PLD) and post-annealing.<br />

The films exhibit sharp superconducting transitions at Tc= 124 K with<br />

transition widths of ∆Tc ≃ 2 K. Conditions for reproducible film preparation<br />

have been found. The resistive transitions have been investigated in<br />

magnetic fields up to 8 T (parallel to the c-axis) and 10 T (perpendicular<br />

to the c-axis). The activation energy of thermally activated flux-motion<br />

has been determined for both magnetic field orientations. The Hall resistivity<br />

(ρxy) has been measured in the ab-plane at 8 T. In the mixed state<br />

a power-law behavior is observed, where ρxy scales to ρxx: ρxy = Aρ β xx,<br />

with β = 1.4 ±0.1. Above 130 K the T 2 dependence of the cotangent of<br />

the Hall angle is observed. Magnetization loops were measured at various<br />

temperatures in a SQUID magnetometer. The corresponding critical cur-<br />

rent densities Jc were calculated. The anisotropic properties of the vortex<br />

state and the depinning field Bdp(θ) have been studied by varying the angle<br />

θ between the field direction and the c-axis of the film. The measured<br />

angular dependence Bdp(θ) shows a cusp for θ = 90 ◦ . The films exhibit<br />

a rather low critical field anisotropy of 7.7. Under the same conditions<br />

(Hg0.9Re0.1)Ba2Ca2Cu3O8+δ (HgRe-1223) thin film (Tc= 130 K) have been<br />

prepared.<br />

TT 8.3 Mo 14:30 Poster A<br />

Novel consideration of the phase diagram of electron doped<br />

high-temperature superductors — •Yoshiharu Krockenberger<br />

1 , Michio Naito 1 , Akio Tsukada 1 , Hideki Yamamoto 1 ,<br />

Lambert Alff 2 , and Rudolf Gross 2 — 1 NTT Basic Research<br />

Laboratories, NTT Corporation, 3-1 Morinosato-Wakamiya, Atsugi-shi,<br />

Kanagawa 243-0198, Japan — 2 Walther-Meissner-Institut, 85748<br />

Garching, Germany<br />

The common phase diagram of high-temperature superconductors<br />

(HTS) including electron doped HTS was published first by Luke et al.[1].<br />

Improved sample quality of hole doped cuprates supported and extended<br />

this phase diagram. Using molecular beam epitaxy it is possible to grow<br />

high quality single phase thin films of electron doped high-temperature<br />

superconductors. Usually, for doping the T ′ -structure tetravalent Ce (e.g.<br />

La2−xCexCuO4+δ) is used. Using trivalent ions instead of Ce 4+ , e.g. Tb 3+ ,<br />

one would expect a Mott insulating and antiferromagnetic state. The caxis<br />

dependence of the doping level as well as XPS measurements clearly<br />

show that the Tb-cation is in the trivalent state. Furthermore, other<br />

trivalent dopants such as Lu, Y, Dy, Eu, and Sm have been investigated<br />

and all of them show the same result: superconductivity below about<br />

20K. This result may shed new light on the usually used phase diagram<br />

of electron doped high temperature superconductors.<br />

[1] G. M. Luke et al., Phys. Rev. B 42, 7981 (1990)<br />

TT 8.4 Mo 14:30 Poster A<br />

Growth and superconducting properties of ternary rare earth<br />

(Gd, Eu, Nd)Ba2Cu3Oy thin films — •C. Cai, J. Hänisch, L.<br />

Fernandez, and B. Holzapfel — IFW Dresden, D-01171 Dresden,<br />

Germany

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