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Symposium X-RAY Magneto-Optics Dienstag Fachsitzungen – Hauptvorträge – SYXM 1 X-Ray Magneto-Optics Zeit: Dienstag 14:30–18:00 Raum: H1 Hauptvortrag SYXM 1.1 Di 14:30 H1 Magneto-optical polarisation spectroscopy with soft x-rays — •Hans-Christoph Mertins 1 , Sergio Valencia 2 , Andreas Gaupp 2 , Wolfgang Gudat 2 , and Peter Oppeneer 3 — 1 University of Applied Sciences, Münster, Stegerwaldstr. 39, 48565 Steinfurt — 2 BESSY, Berlin, Germany — 3 IFW-Dresden, Germany Among the x-ray magneto-optical spectroscopy techniques, the polarisation analysis of light after its interaction with the material gaines increasing importance since it reveals both, the intensity and the phase. Thus it directly gives the complete magneto-optical constants, something that is not possible with a single intensity measurement. Polarisation effects appear when linearly polarized light interacts with a sample that has a magnetization component parallel to the light propagation direction k. Behind the sample the light polarisation plane is rotated and the polarisation has changed to elliptical. This effect has been observed in transmission (Faraday effect [1]) and recently in reflection (L- MOKE [2]). Both effects are even in the magnetization M allowing for investigations of ferromagnetic materials. Antiferromagnetic ordering can be probed by second order effects by applying a perpendicular orientation between k and M (Voigt effect [3]). The applicability of these effects for the characterization of magnetic materials and devices is demonstrated with x-ray rotation and ellipticity spectra across the 3p and 2p edges of Mn, Fe, Co and Ni. [1] J. Kunes et al., Phys. Rev. B 64, 174417 (2001) [2] H.-Ch. Mertins et al., Phys. Rev. B, in press (2003) [3] H.-Ch. Mertins et al., Phys. Rev. Lett. 87, 047401 (2001). Hauptvortrag SYXM 1.2 Di 15:00 H1 Magnetization profiling by resonant magnetic x-ray reflectometry — •G. Schütz, J. Geissler, and E. Goering — Max-Planck Institut für Metallforschung, Stuttgart The asymmetry ratio of resonant magnetic x-ray reflection shows a strong variation with the angle of incidence. The maximum value of the complex magnetic reflection profile is in the order of the corresponding XMCD signal, from which the main magnetic contribution of the absorptive scattering amplitude can be deduced while the dispersive part is calculated via Kramers Kronig relations. If the correlation of the XMCD effect to the atomic magnetic moment is known, the magnetization depth profile can be deduced by an artificial slicing method utilizing the Parratt algorithm [1]. For hard x-rays (e.g. L2,3 edges for 4f or 5d elements) with scattering vector of less than one degree cross and scalar products can be simplified. The application of this theoretical model is much more complicated for soft x-rays and related to large scattering angles. However, this energy range covers the L2,3 edges of 3d transition elements, which exhibit large asymmetry ratios amounting to 50 % [2]. The potential of this method especially for technical relevant GMR/TMR systems, whose magneto-electric properties can strongly depend on the interphase morphogy, is demonstrated for a Pt/Co/Cu trilayer. For this composition it was possible to determine the variation of the magnetic interface depth profile for each layer reaching an accuracy of about 10 % for Pt and Co with a depth resolution up to 0.1 nm. Even for the Cu component an estimation of the induced magnetic moment at the Co-Cu interface is possible [3]. [1] J. Geissler et al., Phys. Rev. B 65, 020405 (2001) [2] J. Geissler et al., Z. Metallkd. 93, 946 (2002) [3] E. Goering et al., in preparation Hauptvortrag SYXM 1.3 Di 15:30 H1 X-ray magneto-optics of lanthanide materials: principles and applications — •José Emilio Prieto, Franziskus Heigl, Oleg Krupin, Kristian Döbrich, Günter Kaindl, and Kai Starke — Institut für Experimentalphysik, Freie Universität Berlin, Germany Lanthanides are frequently employed in technical magnetic systems to achieve high anisotropies. In contrast to transition metals, magnetic moments are carried mainly by the localized 4f electrons, and their correlation energies give rise to rich multiplet structures in optical excitation spectra whenever the 4f shell is involved. This results in strong magnetic dichroism in x-ray absorption and, due to the connection between real and imaginary parts of the refractive index, also in large magneto-optical effects in resonant reflectivity [1]. Soft x-ray magneto-optics is well suited to study magnetization reversal processes in external magnetic fields. Yet in order to obtain quantitative information on the magnetization from reflectivity data, comparison with model calculations is required. Here we report on recent progress in determining the soft x-ray magneto-optical constants of lanthanides [2,3] and show examples of applying specular resonant reflectivity to analyse the magnetization reversal of thin films and exchange-coupled trilayer systems in an element specific way. [1] K. Starke, F. Heigl, A. Vollmer, M. Weiss, G. Reichardt, and G. Kaindl, Phys. Rev. Lett. 86, 3415 (2001) [2] J. E. Prieto, F. Heigl, O. Krupin, G. Kaindl, and K. Starke, Phys. Rev. B 66, 172408 (2002) [3] J. E. Prieto, F. Heigl, O. Krupin, G. Kaindl, and K. Starke, Phys. Rev. B 68, 134453 (2003) Hauptvortrag SYXM 1.4 Di 16:00 H1 Resonant soft x-ray diffuse scattering from magnetic multilayers — •Maurizio Sacchi 1 , Carlo Spezzani 1 , Renaud Delaunay 2 , and Coryn F. Hague 1,2 — 1 LURE, Centre Universitaire Paris Sud, Orsay, France — 2 LCP–MR, Université P. et M. Curie, Paris, France We have applied resonant diffuse scattering of polarized soft x-rays to the investigation of the field dependent magnetic structure in Co/Cu multilayers. At remanence, and for weak applied fields, Co layers break up into magnetic domains with a high degree of AF coupling normal to the stacked layers. We estimate the degree of AF coupling and the average size of the AF domains as a function of the applied field. The analysis of the domain size distribution, and of its correlation with magnetoresistance, after a demagnetization process gives further evidence that the remanent magnetic structure is influenced by the magnetic history of the multilayer. We have compared the field dependence of the sample resistance and of the scattered intensity at various off-specular angles. Our results suggest that at high fields non-negligible variations in the resistance may be due to the persistence of small magnetically hard domains. Hauptvortrag SYXM 1.5 Di 16:30 H1 Ab-initio calculations for adatoms and clusters on surfaces — •Peter H. Dederichs — Institut für Festkörperforschung, Forschungszentrum Jülich, D-52425 Juelich Adatoms and small clusters on surfaces have a considerably lower coordination number than in a bulk environment. Therefore one expects that these nanostructures exhibit considerably larger spin and orbital moments than in the bulk. Here we review a series of ab-initio results for adatoms and small clusters on surfaces of the noble metals (Cu, Ag, Au, Pt) and the ferromagnets Fe and Ni. The calculations were performed within the density-functional formalism by using the KKR-Green’s function method. On the noble metal surfaces, we find strongly enhanced spin moments, and even small clusters of 4d atoms are magnetic. A much stronger enhancement is found for the orbital moments and anisotropy energies. Compared to this, the enhancement of the moments on the surfaces of Fe and Ni are rather moderate, being a result of the much stronger hybridisation of the adatoms with the substrate d states.
Symposium X-RAY Magneto-Optics Dienstag Hauptvortrag SYXM 1.6 Di 17:00 H1 Magnetic properties of mass selected transition metal clusters — •Wilfried Wurth 1 , Leif Glaser 1 , Tobias Lau 1,2 , Michael Martins 1 , Robert Nietuby`c 1 , and Matthias Reif 1 — 1 Institut für Experimentalphysik, Universität Hamburg, Hamburg, Germany — 2 EPFL, Lausanne, Switzerland The magnetism of nanoparticles has attracted a lot of interest recently due to their promising properties for storage media. From a more fundamental point of view small clusters allow to study the transition from the magnetic properties of atoms to those of the respective solids. We have developed a cluster source which enables us to investigate size selected transition metal clusters deposited on solid surfaces using x-ray magnetic circular dichroism. In this talk recent results for iron clusters [1,2] and chromium clusters deposited on ferromagnetic substrates will be presented which demonstrate the strong size dependence of the magnetic properties of the clusters. [1] J.T. Lau, A. Föhlisch, R. Nietuby`c, M. Reif, and W. Wurth, Phys. Rev. Lett. 89, 57202 (2002) [2] J.T. Lau, A. Föhlisch, M. Martins, R. Nietuby`c, M. Reif, and W. Wurth, New J. of Phys. 4, 98.1 (2002) Hauptvortrag SYXM 1.7 Di 17:30 H1 Coherent x-ray scattering and lensless imaging of magnetic materials — •Stefan Eisebitt 1 , Marcus Lörgen 1 , Wolfgang Eberhardt 1 , Jan Lüning 2 , and Joachim Stöhr 2 — 1 BESSY, Berlin, Germany — 2 SSRL, SLAC, Stanford, USA Coherent Scattering is sensitive to the individual sample geometry beyond statistical averages – this is the reason why the speckle fine structure in coherent scattering can be exploited for imaging and to track the dynamics of a sample. The basics of coherent x-ray scattering using synchrotron radiation sources will be reviewed, including advantages and limitations of ”lensless” imaging techniques. Magnetic scattering of soft x-rays and in particular polarization effects in the interference will be discussed in detail, as they have consequences for both static and dynamic studies of magnetic samples. Recent progress in magnetic domain imaging via coherent scattering will be presented. The future perspectives regarding the application of these techniques at free electron x-ray lasers, which will deliver a coherent photon flux many orders of magnitude higher than available today, will be discussed.
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Page 469 and 470: Symposium Life Sciences on the Nano
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