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Symposium Organic and Hybrid Systems for Future Electronics Donnerstag SYOH 4 Hybrid Systems and Devices Zeit: Donnerstag 16:45–17:45 Raum: H37 SYOH 4.1 Do 16:45 H37 Fast integrated plastic circuits — •Robert Blache, Andreas Ullmann, Jürgen Ficker, Dietmar Zipperer, Walt e r Fix, and Wolfgang Clemens — PolyIC GmbH & Co. KG, Paul-Gossen-Str. 100, 91052 Erlangen, Germany Using soluble polymers as active and insulating layers we report on fast and stable integrated circuits based on p-type organic transistors. On flexible polyester film substrates single field-effect transistors and ring oscillators with frequencies above 190 kHz and propagation stage delays below 0.4 µs were fabricated with regioregular poly(3-alkylthiophene). Even without encapsulation the devices show a very stable performance while stored and measured under ambient and extreme conditions [1]. Furthermore we report on organic rectifiers based on polymer rectifier diodes and polymer capacitors. Our results show the potential of integrated plastic circuits based on soluble polymers to be suitable for inexpensive high volume electronic applications (e.g. RFID-tags). [1] J. Ficker, et al., JAP 2003, Vol.94, p. 2638 SYOH 4.2 Do 17:00 H37 Submicron Polymer Field-Effect Transistors — •Susanne Scheinert 1 , Axel Scherer 2 , Theodor Doll 1 , Gernot Paasch 3 , and Ingo Hörselmann 1 — 1 TU Ilmenau — 2 CALTECH, Pasadena, USA — 3 IFW Dresden Application-relevant speed of polymerelectronics requires transistors with submicrometer channel length. At present appropriate low-cost patterning does not exist. We prepared such transistors using a nonlithographic technique for the definition of the channel length in the submicron range. To avoid short-channel effects a hybrid design with silicon dioxide as gate insulator is used. As active layer different poly(3alkythiophene) (P3AT) has been used. The transistors feature (i) controlled defined channel length between 0.75µm and 1µm, (ii) an operation at voltages lower than 5V , (iii) well pronounced saturation of the output characteristics with (iv) only marginal short channel effects, (v) a high on-off ratio (> 10 4 ), (vi) rather small inverse subthreshold slope S ≈ 0.5V/dec, and (vii) negligible contact resistances. Since the used P3AT were not especially treated, the mobility is still low (≈ 2...3cm 2 /V s). The hysteresis is negligible for the drain voltage sweep for a given gate voltage, but as usual there is a hysteresis for the gate voltage sweep at given drain voltage. However, the corresponding threshold voltage shift is with ≈ 1V relatively small. SYOH 5 Poster SYOH 4.3 Do 17:15 H37 Cascade energy transfer in bandgap modulated multilayer structures of CdTe quantum dots — •Thomas Franzl, Stefan Schietinger, Thomas A. Klar, Andrey L. Rogach, and Jochen Feldmann — Photonics and Optoelectronics Group, Physics Department and CeNS, Ludwig-Maximilians-Universität München, Amalienstr. 54, D-80799 Munich, Germany We report on very fast and directed energy transfer leading to strongly increased excitonic densities in cascaded energy transfer structures (CET) made of CdTe quantum dots capped by short chain thiols. A systematic bandgap variation in one spatial direction is realized by a layer-by-layer technique using CdTe nanocrystals of stepwise increasing sizes in subsequent layers. We observe an efficient energy transfer towards the layer of largest quantum dots. In this layer the excitonic density increases by an order of magnitude in comparison to a layered system containing only one size of CdTe nanocrystals. These high excitonic densities in CET structures are especially interesting for optoelectronic devices such as nanocrystal LEDs or lasers. SYOH 4.4 Do 17:30 H37 Optical modeling of CuPc/C60 photovoltaic devices — •T. Stübinger 1 and W. Brütting 2 — 1 Experimentalphysik II, Universität Bayreuth, D-95440 Bayreuth — 2 Experimentalphysik IV, Universität Augsburg, D-86135 Augsburg Photovoltaic devices with Cu-phthalocy anine (CuPc) as electron donor and Buckminsterfullerene (C60) as electron acceptor exhibit high incident photon-to-current conversion efficiencies (IPCE) in bilayer devices and composite systems. Optical interference effects significantly influence photocurrent spectra and quantum efficiencies, which arises from the strong dependence of layer thicknesses on the spatial distribution of the photon density. By optical modelling using transfer-matrix-methods the experimental photocurrent spectra of bilayer systems with various layer thicknesses (organic layers, buffer layers, electrodes) could be explained. Blend systems of CuPc and C60 show high quantum efficiencies of almost 60% (IPCE) due to an effectively enhanced dissociation volume in these composite systems. These high IPCE values demonstrate a very efficient photocarrier generation and charge transport in these low molecular weight composite systems, which is comparable to the most efficient polymer-fullerene composite systems after post-annealing treatments. The mixing ratio and total layer thickness of the blend system are varied to achieve optimum photovoltaic performance. Zeit: Donnerstag 18:00–21:00 Raum: B SYOH 5.1 Do 18:00 B Normal Incidence X-ray Standing Waves on Light Elements: The Limits of the Dipole Approximation — •Christian Kumpf, Jörg Stanzel, Christoph Stadler, Wolfgang Weigand, and Eberhard Umbach — Experimentelle Physik II, Univ. Würzburg The normal incidence x-ray standing wave (NIXSW) technique is a powerful tool for obtaining detailed structural information on surfaces, e.g., exact atomic coordinates which enable quantum chemical calculations. In most XSW experiments either the photoelectron or the Augerelectron yield is used to measure the absorption of a specific atomic species adsorbed on a surface. For the analysis of organic adsorbates, which contain low-Z elements only, this is a difficult issue since the dipoleapproximation is no longer sufficient to describe the photoemission process. Using the Auger yield is also problematic since the Auger process is not only stimulated by the x-ray standing wave field but also by (photo-) electrons emerging from the bulk. Therefore, significant effort was put in finding a proper way to correct the photoemission yield for non-dipolar contributions as well as the Auger-yield for its electron-induced portion. We report on a NIXSW experiment performed on a coherent monolayer of NTCDA on Ag(111) for which this correction was successfully performed and consistent results were obtained from the O1s photo electron yield as well as from the OKLL Auger electron yield. The electroninduced portion of the Auger yield was found to be as large as 50%. Furthermore, a significant covalent character was found for the bonding between the NTCDA molecules and the substrate. The bonding distance is 3.08(3)˚A, considerably smaller than a Van der Waals distance. SYOH 5.2 Do 18:00 B Template guided self-assembly of nanoclusters — •Li Zhang, Lifeng Chi, and Harald Fuchs — Physikalisches Institut, Westfälische Wilhelms-Universität, Wilhelm-Klemm-Str. 10, 48149 Münster, Germany Surface patterning with microscopically small structures has attracted increasing scientific and technological interest over the past decade. In our work, variable surface patterns of chiral molecule C11-CO-(L)-Cys- (L)-Cys-NH-C18 are obtained by changing the subphase conditions. At the air- water (pure) interface, it forms a kind of chiral pattern. Due to the potential complex ability of the sulfur atom in the molecule, this kind of surface aggregate could be used as a template to trap the metal ions or nanoparticles during its interfacial assembly process, which may provide a method to assemble the metal or semi-conductor particles into a designed way. Using the metal ions as subphase, the chiral pattern size is smaller compared with the result without metal ions. The size of this kind of aggregate decreases with increased concentration of metal ions. For the subtle structure inside the circle domain, the stripe like structure is found. At the air-CdTe nanoparticle aqueous interface, a kind of branched nanostripes appears. The furcation point appears at the end of some branches.
Symposium Organic and Hybrid Systems for Future Electronics Donnerstag The preliminary results of SEM and confocal fluorescence microscopy show that the nanoparticle are trapped in the nanowires during the process of interfacial assembly. SYOH 5.3 Do 18:00 B STM Investigation of the Adsorption of C60 Molecules on Vicinal Si(111)-7x7 Surfaces — •Yu Suzuki, Falk Müller, Thorsten Kampen, Michael Hietschold, and Dietrich Zahn — Institute of physics, University of Technology Chemnitz, 09126 Chemnitz, Germany Vicinal silicon surfaces have attracted much attention as promising candidates for templates of self-assembled organic nano-structures. The step edges on vicinal surfaces might serve as preferential adsorption sites for the molecules, which may result in the self-assembly of molecular nano-wires. In this study the adsorption of high symmetrical C60 on vicinal Si(111)- 7x7 surfaces was investigated using scanning tunnelling microscopy under UHV conditions. The vicinal silicon substrates were first chemically cleaned by hydrogen peroxide and followed by direct current heating in UHV. STM showed stepped surface on vicinal silicon after this preparation procedure. A 7x7 reconstruction was confirmed by LEED and STM. However, the morphology of the vicinal surfaces were strongly affected by details of the preparation procedure. The C60 molecule at the edges showed more stability and less mobility against the manipulation by STM tip, compared to the ones on terraces of silicon steps. SYOH 5.4 Do 18:00 B Self-assembly of highly rigid redox-active nanostructures monitored by optical second harmonic generation — •Tobias Weidner 1 , Jens Vor der Brüggen 2 , Andreas Krämer 2 , Ulrich Siemeling 2 , and Frank Träger 1 — 1 Institut für Physik and Center for Interdisciplinary Nanostructure Science and Technology - CINSaT, Universität Kassel, Heinrich-Plett-Str. 40, D-34132 Kassel — 2 Institut für Chemie and Center for Interdisciplinary Nanostructure Science and Technology - CINSaT, Universität Kassel, Heinrich-Plett-Str. 40, D-34132 Kassel We have used self-assembly techniques for the preparation of highly ordered electronically active monolayers on gold substrates. Many compounds used for self assembly at present are intrinsically flexible due to flexible spacer units thus limiting the overall film ordering. To resolve this problem we have synthesized compounds bearing highly rigid π-spacers and 2, 2 ′ : 6 ′ , 2 ′′ -terpyridin-4 ′ -yl or tripodal tris[(methylthio)methyl]silyl headgroups, adding to the rigidity of the obtained films. These molecules have been functionalised with phenyl and ferrocenyl groups. Ferrocene is a redox-active organometallic unit which is widely used for sensoric and electronic applications. Adsorption from solution was studied in situ by optical second harmonic generation (SHG) with submonolayer resolution. SHG was also used to examine film ordering in real time. The results have been compared to ellipsometric measurements. The data show that adsorption leads to the formation of monomolecular films at the interface. We found that film growth is followed by self-assembly of highly ordered redox-active ferrocenyl nanostructures. SYOH 5.5 Do 18:00 B Luminescence quenching of tetracene molecules adsorbed on the sapphir surface — •Andreas Langner and Moritz Sokolowski — Institut für Physikalische und Theoretische Chemie, Universität Bonn, Wegelerstr. 12, D-53115 Bonn A surface usually affects the photolumenescence (PL) of adsorbed molecules. Our aim is to understand the mechanisms which modify the PL, in order to apply PL spectroscopy to learn something about the dynamic processes of molecules on surfaces (e.g., mobility, diffusion, rotation of molecules). So far PL investigations of isolated molecules on well defined surfaces are missing, partly because on metallic surfaces ultrafast quenching occurs and no fluorescence is observable. However, on surfaces of wide gap insulator materials we expect to obtain PL signal from adsorbed molecules. In particular, we have investigated tetracene evaporated at 100K on Al2O3(0001). The substrate was prepared in UHV by Ar + sputtering and annealing in O2 at 1200K. We control the number of adsorbed molecules very accurately by thermal desorption. Contrary to our expectation, no fluorescence is observed for a 0.2 monolayer thick film of presumably isolated molecules. After annealing to 240K we can measure an increase of the PL signal of the order of three magnitudes, which is probably due to the growth of 3Dtetracene-crystallites. We report the evolution of the PL in dependence of the film thickness and the annealing temperature. SYOH 5.6 Do 18:00 B Langmuir-Blodgett monolayer behavior of dinuclear ruthenium(II)trisbipyridine complexes — •Xiaodong Chen 1 , Frank Vergeer 2 , Steve Welter 2 , Luisa de Cola 2 , Lifeng Chi 1 , and Harald Fuchs 1 — 1 Physikalisches Institut, Wilhelm-Klemm-Str. 10, 48149, Muenster, Germany — 2 Molecular Photonics Group, Institute of Molecular Chemistry, University of Amsterdam, 1018 WV Amsterdam, The Netherlands Dinuclear ruthenium complexes have been generating interest as a class of electroluminescent materials [1]. Langmuir-Blodgett (LB) technique is a powerful tool for assembling different molecules to build ultrathin organic films with well-controlled structure and thickness. In the present report, we used the LB technique to prepare dinuclear ruthenium(II)trisbipyridine complexes monolayers. The complexes contain two Ru(bpy) 2+ 3 moieties and four phenylene units as spacers between the two ruthenium centers. From the surface pressure-molecular area isotherms and morphologies, it was found that the complexes possessing long alkyl chains on one of the Ru(bpy) 2+ 3 centers and those without long alkyl chains show different behaviors. It seems that the introduction of the alkyl chains in the complexes is indeed necessary to obtain a more homogeneous film. In addition, the effect of pressure on the morphologies of monolayers was considered. The results provide basic clues for future monomolecular layers electroluminescent device preparation. [1] S. Welter et al. Nature 421, 54 (2003) SYOH 5.7 Do 18:00 B Synthese von molekularskaligen Drähten auf DNA-Basis — •Patrick Nickels, Wendy Huynh und Friedrich Simmel — Sektion Physik und Center for Nanoscience, Universität München, Geschwister-Scholl-Platz 1, 80539 München Die herausragenden molekularen Erkennungseigenschaften von DNA- Molekülen können für den Aufbau komplexer supramolekularer Netzwerke genutzt werden. Solche Netzwerke könnten die Grundlage selbstorganisierter Schaltkreise bilden. Die unzureichenden elektronischen Eigenschaften von DNA-Molekülen verhindern allerdings ihren unmittelbaren Einsatz als molekularskalige Komponenten. Ein wesentlicher Schritt ist daher die Funktionalisierung von DNA-Strängen mit halbleitenden oder metallischen Materialien. Hier präsentieren wir verschiedene Methoden zur DNA-gesteuerten Synthese von Metallen, leitfähigen Polymeren und anorganischen Halbleitern sowie deren rasterkraftmikroskopische und elektronische Charakterisierung. SYOH 5.8 Do 18:00 B Self-Organized Nanocomposites of CdSe Nanocrystals and Porphyrins — •Abey Issac 1 , Thomas Blaudeck 2 , Frank Cichos 2 , Edward Zenkevich 3 , Alexander Shulga 3 , and Christian von Borczyskowski 1 — 1 Institut für Physik 122501, TU Chemnitz, 09107 Chemnitz — 2 Institut für Physik 123705, TU Chemnitz, 09107 Chemnitz — 3 Institute of Molecular and Atomic Physics and B.I. Stepanov Institute of Physics National Academy of Sciences, 70 F. Skaryna Avenue, 220072 Minsk, Belarus Composites of semiconductor nanocrystals (NC) and organic compounds open a road to new functional units for optoelectronic applications. Such composites may be prepared by self-organization of functionalized organic chromophores on semiconductor NCs. We present results of spectroscopic studies, where we investigate composites of pyridyl containing porphyrin molecules and CdSe NCs in solution. The experiments show a strong quenching of the emission of CdSe NCs even at ratios of the porphyrin to NC concentration much smaller than one. This is ascribed to the self-organization of porphyrin molecules on the NC surface by ligation interactions. The close proximity of NC and porphyrin and their electronic interaction opens nonradiative channels, which we tentatively ascribe to an electron transfer process from the NC to the porphyrin. With increasing number of porphyrin molecules per NC the NC emission is quenched almost completely. This points to an electron transfer, that occurs on a much shorter timescale than the emission decay of the NC which is confirmed by time resolved measurements. The dependence of the observed emission quenching on the NC size will be discussed. SYOH 5.9 Do 18:00 B Nanopatterning of Organically Modified Semiconductor Surfaces — •Thierry Djenizian, Eugen Balaur, Yan Zhang, and Patrik Schmuki — Chair for Surface Science and Corrosion, WW4, University of Erlangen-Nuremberg, Martensstrasse 7, 91058, Erlangen The preparation, development and integration of practical electronic
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Page 485 and 486: Symposium Functional Nanoparticles
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Page 489: Symposium Organic and Hybrid System
Page 507 and 508: Symposium Physics of Foams Mittwoch
Page 509 and 510: Symposium Physics of Foams Mittwoch
Page 511 and 512: Symposium Quantum Shot Noise in Nan
Page 513 and 514: Symposium X-RAY Magneto-Optics Tage
Page 515 and 516: Symposium X-RAY Magneto-Optics Dien
Page 517 and 518: Lehrertage Regensburg Hauptvorträg
Page 519 and 520: A. D., Mirlin .................HL 1
Page 521 and 522: Breidenbach, Boris ........ AKB 50.
Page 523 and 524: Elli, Alexandra .............SYLS 3
Page 525 and 526: Greer, Lindsay ......... M 9.1, M 1
Page 527 and 528: Horn-von Hoegen, M. O 13.2, O 14.40
Page 529 and 530: Korn, Tobias ...............MA 13.6
Page 531 and 532: Martin, Tobias ............. MA 13.
Page 533 and 534: Partyka, Ewa ................ M 18.
Page 535 and 536: Rugeramigabo, Eddy Patrick O 14.38,
Page 537 and 538: Sihler, J. .................... DS
Page 539 and 540: Volz, K. .................... HL 44
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