Angelika Semmler - KOPS - Universität Konstanz

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8 Experimenteller Teil
Cyclo[Met(O)-Gly-Ala-Pro-Gly-Phe-Glu(-βAla-Pro-Pro-Arg(Pbf)-N-(4-Bromphenyl-
MALDI-TOF-MS: 1351,9 m/z [M+H] +
Berechnet: C59H84BrN16O18S + (1351,5252 m/z)
Peptid (43→44)
H-Gly-Ala-Pro-Gly-Phe-Glu(-βAla-Pro-Pro-Arg-OH)-Hsl
MALDI-TOF-MS: 1152,9 m/z [M+H] +
Berechnet: C52H78N15O15 + (1152,5796 m/z)
H-Gly-Ala-Pro-Gly-Phe-Glu(-βAla-Pro-Pro-Arg-N-(4-Bromphenylamid))-Hsl
MALDI-TOF-MS: 1305,9 m/z [M+H] +
Berechnet: C58H82BrN16O14 + (1305,5374 m/z)
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