Angelika Semmler - KOPS - Universität Konstanz

H-Lys-Gln-Pro-His-His-Gly-Glu-βAla-Pro-Pro-Arg-NH2 (97)
Analytische RP-HPLC: (8-30% B in 45 min) tR = 12,3 min
ESI-QTOF: 1252,6663 m/z (±0,4 ppm)
Berechnet: C54H86N21O14 + (1252,6658 m/z)
mAU
400
214nm,4nm (1.00)
350
300
250
200
150
100
50
0
-50
-100
0
0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 40.0 45.0 min
Intens.
x104
2.0
1.5
1.0
0.5
0.0
Intens.
x104
2.0
1.5
1.0
0.5
0.0
1097.5973
1234.6558
12.286
%
B.Conc.(Method)
10 Anhang
90
80
70
60
50
40
30
20
10
+MS, 1.7min #103
1000 1500 2000 2500 3000 3500 4000 4500 5000m/z
1234.6558
1250.6365
1256.6369
1272.6121
+MS, 1.7min #103
1230 1240 1250 1260 1270 1280 m/z
177