ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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Creating an Instrument Control Method 169 Direct Control Temperature (°C) The oven temperature can be set. The entered value will be transferred to the oven by clicking the Set button. Cooler Temperature (°C) (S 4050 only) The oven temperature can be set. The entered value will be transferred to the oven by clicking the Set button. Leakage Alarm Level (%) (S 4050 only) The leakage alarm level can be set. The entered value will be transferred to the oven by clicking the Set button. Digital Outs (Events) (S 4050 only) Click on the button to set up the digital outputs. Refer to the chapter described in the chapter Instrument Setup – Pumps, section Configuring Digital Outputs for details. Click the DO Apply button to accept the settings. Set Temperature Control (S 4050 only) Press the Off button to switch the temperature control off. It will be switched on again by setting the desired temperature and pushing the Set button. GLP (S 4050 only) The minimum and maximum reached temperatures, the total working time and the working time above 150°C will be monitored. The read out will be actualized by clicking on the Refresh button. Instrument Status – Flowmeter Fig. 248 Status tab, Knauer Flowmeter Monitor Run Status The status HOLD will be displayed when no program is running; otherwise the Run Status displays a run time in minutes elapsed from the start of the run. Flow (ml/min) The actual flow will be shown in units as defined in the instrument setup.
170 Knauer Instrument Control Method Options Knauer Instrument Control Method Options General Settings Some general method settings belong exclusively to the Knauer instrument control. They are accessible by the METHOD menu. Runtime Settings The runtime setting options are general settings. The selection is valid for all ChromGate methods until it is changed. Fig. 249 Knauer Instrument Control Method Option - Runtime Settings Emergency during a run options In the case that an emergency situation is detected, the software can be forced to stop all pumps and/or to switch off all lamps and/or switch off all ovens. If enabled, this option is valid for the currently used computer. Direct Control during a run If this option is enabled, all devices can be controlled manually using the Direct control section of the device’s instrument status tab. The direct control during a run option is a valuable tool for method development but can also lead to the possibility for unintended changes to the method. For this reason, it is recommended that this option not be enabled, especially for routine methods. All changes during a run will be added to the instrument activity log, but cannot be stored in the original/acquisition method, attached to the data file. This may not meet your GLP/GMP requirements. Save Changes in time table This option can only be enabled/disabled, if the “Enabled” checkbox for “Direct Control during a run” is activated. If the “Save changes…”-Option is checked, any method changes by direct control will be saved in the method. Otherwise the changes only can be monitored in the instrument activity log and in the audit trail, refer to the EZChrom reference manual. Due to that the changes cannot be stored in the method, which is attached as the original/acquisition method to the data file; we recommend reanalyzing the chromatogram with the changed method. All methods used to analyze a chromatogram, also will be added to the chromatogram data file and can be extracted as “From Results” in the Open Data dialog.
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Software ChromGate ® Chromatograph
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4 CONTENTS Configuration - Autosamp
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6 CONTENTS Peak Table .............
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8 Installation Guide ChromGate® 3.
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10 Installation Guide ChromGate® 3
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12 Installation Guide ChromGate® 3
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14 Short guide ChromGate®, KNAUER
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32 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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220 ChromGate® PDA Option Fig. 318
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222 PDA Analysis and Calculations c
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224 PDA Analysis and Calculations s
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226 PDA Analysis and Calculations u
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228 PDA Analysis and Calculations 3
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230 ChromGate® Preparative Option
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258 SEC Option Universal Calibratio
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260 SEC Option Fig. 369 Acquisition
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262 SEC Option Amount Values In thi
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264 SEC Option Fig. 373 SEC peak an
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266 SEC Option Fig. 376 Fig. 377 Yo
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268 SEC Option Fig. 379 Enable Anal
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270 SEC Option Export settings Clic
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272 SEC Option All samples analyzed
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274 SEC Option Horizontal Baseline
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276 SEC Option Intrinsic Viscosity
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278 SEC Option Fig. 383 information
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280 SEC Option Fig. 386 Fig. 387 Se
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282 SEC Option single variable sear
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284 Typical Wiring Schemes Typical
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286 Typical Wiring Schemes Fig. 390
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288 Typical Wiring Schemes Fig. 392
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290 Fig. 394 Pump K-1001 / Autosamp
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292 Index Device ID Autosampler 68,
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294 Index R Rack configuration 243
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