ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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CONTENTS 3 CONTENTS Installation Guide ChromGate ® 3.3.2 ............................................................................... 8 General Definitions .................................................................................................... 8 Installation .................................................................................................................. 8 KNAUER FRC control option ...................................................................................11 Short Guide ChromGate ® , KNAUER Instrument Control .............................................13 Overview .......................................................................................................................13 Configuring a System ...................................................................................................14 Instrument Configuration .........................................................................................14 System Options .......................................................................................................14 Setting up a Method ......................................................................................................15 The Instrument Wizard ............................................................................................15 The Method Window ................................................................................................16 Quantification of the Compound(s) of Interest ..............................................................19 Overview ..................................................................................................................19 Integration ................................................................................................................19 Generating and Using a Calibration Curve ..............................................................20 Method File Commands ................................................................................................20 Quantification and Using Sequence Files .....................................................................20 Overview ..................................................................................................................20 Single Level Calibration ...........................................................................................21 Creating a Sample Sequence ..................................................................................23 Running a Sequence ...............................................................................................25 Reporting .................................................................................................................26 Collecting Data ..............................................................................................................28 General Data Collection Instructions with ChromGate ............................................28 Collecting Data ........................................................................................................28 Instrument Status of a running Control Method .......................................................29 Shutting Down the System ...........................................................................................30 Setup and Control of Knauer HPLC Systems ...............................................................31 Overview of Instrument Control ....................................................................................31 Configuration – device communication port ............................................................31 Configuring the Interface .........................................................................................31 Knauer Interface Configuration ................................................................................32 Kontron Interface Configuration ...............................................................................34 K-2700 / 2800 Interface Card and Driver Installation ..............................................35 Configuring the KNAUER HPLC System .................................................................35 Instrument Configuration ..............................................................................................36 Configuration – KNAUER HPLC System .................................................................36 Configuration – Knauer Pumps................................................................................38 Configuration – Kontron Pumps...............................................................................44 Configuration – Knauer Detectors ...........................................................................45 Configuration – User Defined Detectors ..................................................................53 Configuration – Kontron UV-Detectors ....................................................................55 Configuration – Kontron Diode Array Detectors ......................................................56 Configuration – Virtual Detector...............................................................................57 Detector Connections ..............................................................................................57 Configuration – Assistant ASM2.1L .........................................................................60 Configuration – Autosampler ...................................................................................63 Configuration – Autosampler 3950 ...........................................................64
4 CONTENTS Configuration – Autosampler Knauer Optimas ........................................ 67 Configuration – Autosampler 3800 .......................................................... 70 Configuration – Autosampler 3900 .......................................................... 71 Configuration – Autosampler Triathlon / Endurance ............................... 72 Configuration – Kontron Autosamplers ................................................... 76 Configuration – Miscellaneous Instruments ............................................................ 78 Configuration – Switching Valves ............................................................ 78 Configuration – Manager 5000/5050, IF2 ................................................ 79 Configuration – Column Oven 4050, Column Oven Jetstream ............... 80 Configuration – Flowmeter ...................................................................... 81 Creating an Instrument Control Method ....................................................................... 83 Instrument Setup .......................................................................................................... 84 Instrument Setup – Pumps ..................................................................................... 85 Instrument Setup – Detectors ................................................................................. 91 All Detectors 91 Instrument Setup – RI Detectors ............................................................. 92 Instrument Setup – UV Detectors (S 200, K-200) ................................... 92 Instrument Setup – UV Detectors (K-2000, K-2500) ............................... 92 Instrument Setup – UV Detectors (UVD 2.1L, UVD 2.1S, S 2520, S 2500, K-2001, K-2501) ............................................. 93 Instrument Setup – Kontron Detectors .................................................... 95 Instrument Setup – K-2600 Detector ....................................................... 95 Instrument Setup – S 2550 Detector ....................................................... 98 Instrument Setup – Diode Array Detectors (S 2600, DAD 2850, DAD 2800, K-2700 and Kontron DAD 540/545) ... 100 Instrument Setup – Fluorescence Detector RF-10Axl / RF-20A ........... 103 Instrument Setup – Alltech 650 Conductivity Detector .......................... 104 Instrument Setup – User defined Detector ............................................ 104 Instrument Setup – Virtual Detector ...................................................... 105 Instrument Setup – Assistant ASM2.1L ................................................................ 107 Instrument Setup – Autosamplers......................................................................... 111 Instrument Setup – Autosampler 3800 .................................................. 111 Instrument Setup – Autosampler Knauer Optimas / 3900 (Midas)........ 112 Instrument Setup – Autosampler 3950 (Alias) ....................................... 116 Instrument Setup – Triathlon/Endurance Autosampler ......................... 121 Instrument Setup – Kontron Autosamplers ........................................... 128 Instrument Setup – Miscellaneous Instruments .................................................... 130 Instrument Setup – Manager 5000/5050/IF2 I/O ................................. 130 Instrument Setup – Switching Valves .................................................... 131 Instrument Setup – Column Oven 4050 ................................................ 133 Instrument Setup – Column Oven Jetstream ........................................ 133 Instrument Setup – Flowmeter .............................................................. 134 Setting up Auxiliary Traces ................................................................................... 135 Setting up a Trigger .............................................................................................. 135 Setting up the Baseline Check .............................................................................. 136 Instrument Status of a (running) Control Method ....................................................... 137 System Status ....................................................................................................... 137 Instrument Status – Pumps ................................................................................... 139 Instrument Status – Detectors .............................................................................. 145 Instrument Status – RI Detectors (S 23[4]00, K-23[4]00/1) ................... 145 Instrument Status – UV Detectors (S 2520, S 2500, S 200, K-200, K- 2000/1, K-2500/1) ......................................... 145 Instrument Status – Kontron Detectors (3xx, 4xx, and 5xx) .................. 147 Instrument Status – fast scanning UV Detector (K-2600) ..................... 148 Instrument Status – Diode Array Detectors ........................................... 149 Instrument Status – Fluorescence Detector RF-10Axl / RF-20A .......... 152 Instrument Status – Conductivity Detector Alltech 650 ......................... 154 Instrument Status – User Defined Detector ........................................... 154
Page 1: Software ChromGate ® Chromatograph
Page 5 and 6: 6 CONTENTS Peak Table .............
Page 7 and 8: 8 Installation Guide ChromGate® 3.
Page 9 and 10: 10 Installation Guide ChromGate® 3
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Page 13 and 14: 14 Short guide ChromGate®, KNAUER
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54 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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170 Knauer Instrument Control Metho
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186 ChromGate® System Suitability
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188 ChromGate® System Suitability
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190 ChromGate® PDA Option Fig. 283
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192 ChromGate® PDA Option calculat
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194 ChromGate® PDA Option (to the
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196 ChromGate® PDA Option PDA View
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216 ChromGate® PDA Option Note tha
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222 PDA Analysis and Calculations c
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224 PDA Analysis and Calculations s
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226 PDA Analysis and Calculations u
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228 PDA Analysis and Calculations 3
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230 ChromGate® Preparative Option
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258 SEC Option Universal Calibratio
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260 SEC Option Fig. 369 Acquisition
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262 SEC Option Amount Values In thi
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264 SEC Option Fig. 373 SEC peak an
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266 SEC Option Fig. 376 Fig. 377 Yo
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268 SEC Option Fig. 379 Enable Anal
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270 SEC Option Export settings Clic
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272 SEC Option All samples analyzed
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274 SEC Option Horizontal Baseline
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276 SEC Option Intrinsic Viscosity
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278 SEC Option Fig. 383 information
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280 SEC Option Fig. 386 Fig. 387 Se
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282 SEC Option single variable sear
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284 Typical Wiring Schemes Typical
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286 Typical Wiring Schemes Fig. 390
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288 Typical Wiring Schemes Fig. 392
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290 Fig. 394 Pump K-1001 / Autosamp
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292 Index Device ID Autosampler 68,
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294 Index R Rack configuration 243
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ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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