ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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ChromGate® Preparative Option 251 selected, click on the -button. The pump configuration window will open. Please configure the pump accordingly the pump configuration described in the appropriate chapter. Note that you cannot configure the same pump as for the solvents. However, it is not possible to use e.g. one channel of an LPG solvent pump for the injection module. Also configure the valve as described in the appropriate chapter. If you want to use a sample loop, enable the check box Use Sample Loop. The injection module also allows for using the AZURA ASM 2.1L as an injection module, if a pump and a valve have been installed. The installed modules in the ASM 2.1L have own IP ports, which allows for separate control. The configuration does to allow to select an ASM 2.L or search for the modules by using the -button – the pump and valve must be configured in the Injection Module configuration manually. To use an ASM-pump or -valve in the injection module, select the appropriate pump or valve model in the Injection Module configuration, disable the option “Use S/N to identify the instrument” and enter manually the serial number and IP address of the ASM 2.1L device. Now change the IP port for the modules (pump and valve): If the ASM 2.1L has IP port 10001, the module installed on the left side has IP port 10002, the middle module 10003 and the module installed on the right-handed side the IP port 10004. If the IP port of the ASM 2.1L has been changed in the ASM’s own setup, the IP ports of the build-in modules will be changed automatically; they will always have the next possible IP ports. However, before you enter the IP ports of the pump and valve, please check for the IP port of the used ASM 2.1L device. Injection module instrument setup If you open the configured instrument and the instrument setup, you will find an own tab for the injection module. Fig. 360 Injection module instrument setup window The injection module will be used for the initial and the stacked injections. Injection program The settings in this section will only be used for the initial injection, that means, for the first injection at the start of the run. Injection Volume Enter the desired injection volume in ml. Injection Flow
252 ChromGate® Preparative Option Enter the flow rate of the injection pump during the injection. If no injection is prepared, the pump is stopped; during a run the pump and valve cannot be controlled beside the programmed stacked injection. Injection Duration The duration of the injection is calculated from the injection volume and the injection flow. The reduced flow during start and stop of the pump is taken into account with 6 seconds in sum. Pump Settings Control Pressure Limits (MPa) Enter the values for the desired pressure limit. 0 will disable the software control of the pressure. Keep in mind that the pressure for the sample loading may be different from the system pressure during a run if a different flow rate is used or if you use a sample loop. Note that for a pump S 100 without pressure transducer this option is not accessible. Solvent Enter the name of the solvent. Stacked Injections [>>…] The option Stacked injections allow to define additional injections during a run. Such injections can be programmed either for the autosampler 3950 or the injection module (please refer the Instrument Setup for the autosampler 3950 for details of the stacked Injection setup of the autosampler. Click on the [>>…] – button to open the Stacked Injections table dialog. Fig. 361 Injection module Stacked injection table Stacked injections time table Make a right mouse click into the time table and select Fill table from the corresponding menu. Fig. 362 Injection module Stacked injections table setup
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Software ChromGate ® Chromatograph
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4 CONTENTS Configuration - Autosamp
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6 CONTENTS Peak Table .............
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8 Installation Guide ChromGate® 3.
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10 Installation Guide ChromGate® 3
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12 Installation Guide ChromGate® 3
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14 Short guide ChromGate®, KNAUER
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32 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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170 Knauer Instrument Control Metho
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186 ChromGate® System Suitability
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188 ChromGate® System Suitability
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190 ChromGate® PDA Option Fig. 283
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192 ChromGate® PDA Option calculat
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194 ChromGate® PDA Option (to the
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196 ChromGate® PDA Option PDA View
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198 ChromGate® PDA Option Fig. 291
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Page 221 and 222: 222 PDA Analysis and Calculations c
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Page 225 and 226: 226 PDA Analysis and Calculations u
Page 227 and 228: 228 PDA Analysis and Calculations 3
Page 229 and 230: 230 ChromGate® Preparative Option
Page 249: 250 ChromGate® Preparative Option
Page 257 and 258: 258 SEC Option Universal Calibratio
Page 259 and 260: 260 SEC Option Fig. 369 Acquisition
Page 261 and 262: 262 SEC Option Amount Values In thi
Page 263 and 264: 264 SEC Option Fig. 373 SEC peak an
Page 265 and 266: 266 SEC Option Fig. 376 Fig. 377 Yo
Page 267 and 268: 268 SEC Option Fig. 379 Enable Anal
Page 269 and 270: 270 SEC Option Export settings Clic
Page 271 and 272: 272 SEC Option All samples analyzed
Page 273 and 274: 274 SEC Option Horizontal Baseline
Page 275 and 276: 276 SEC Option Intrinsic Viscosity
Page 277 and 278: 278 SEC Option Fig. 383 information
Page 279 and 280: 280 SEC Option Fig. 386 Fig. 387 Se
Page 281 and 282: 282 SEC Option single variable sear
Page 283 and 284: 284 Typical Wiring Schemes Typical
Page 285 and 286: 286 Typical Wiring Schemes Fig. 390
Page 287 and 288: 288 Typical Wiring Schemes Fig. 392
Page 289 and 290: 290 Fig. 394 Pump K-1001 / Autosamp
Page 291 and 292: 292 Index Device ID Autosampler 68,
Page 293 and 294: 294 Index R Rack configuration 243
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