ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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CONTENTS 5 Instrument Status – Virtual Detector ......................................................155 Instrument Status – Assistant ASM2.1L ................................................................156 Instrument Status – Autosampler ..........................................................................161 Instrument Status – Autosampler 3800 ..................................................161 Instrument Status – Autosampler Optimas/3900 ...................................162 Instrument Status – Autosampler 3950 ..................................................163 Instrument Status – Triathlon/Endurance Autosampler .........................165 Instrument Status – Kontron Autosamplers ...........................................166 Instrument Status – Miscellaneous Instruments ....................................................166 Instrument Status – Manager 5000/5050/IF2 I/O ..................................166 Instrument Status – Knauer Switching Valves .......................................167 Instrument Status – Column Oven 4050 and Jetstream ........................168 Instrument Status – Flowmeter ..............................................................169 Knauer Instrument Control Method Options ...............................................................170 General Settings .........................................................................................................170 Runtime Settings ...................................................................................................170 Download Tab / Method .........................................................................................172 Solvent Control ......................................................................................................173 Qualification Procedures .............................................................................................175 Validation of Integration ..............................................................................................178 Generic Drivers ...........................................................................................................183 ChromGate ® System Suitability Setup .........................................................................185 Copy & Paste .........................................................................................................186 Suitability Calculation Selection .............................................................................186 Running a Suitability Test ......................................................................................187 Suitability Reports ..................................................................................................188 ChromGate ® PDA Option...............................................................................................189 PDA Method Setup .....................................................................................................189 PDA Options Library ..............................................................................................189 PDA Options Purity ................................................................................................191 PDA Options Spectrum ..........................................................................................192 PDA Options Multi-Chromatogram ........................................................................194 PDA Options Ratio .................................................................................................195 PDA Views ..................................................................................................................196 3D View ..................................................................................................................196 Contour View .........................................................................................................199 Mixed View.............................................................................................................203 Chromatogram View ..............................................................................................204 Spectrum View .......................................................................................................208 Ratio View ..............................................................................................................210 Spectrum Similarity Table ......................................................................................211 Spectral Library Definition ......................................................................................212 How to Collect Spectra for a Library ......................................................................213 How to Add Spectra to a Library ............................................................................213 Library Search .......................................................................................................214 Spectral Library Search .........................................................................................214 Custom Report ............................................................................................................216 PDA Insert Graph Items .........................................................................................216 PDA Insert Report Items ........................................................................................217 Library Search Report 217 Library Definition Report 218 Spectrum Report 219 Spectral Display 221
6 CONTENTS Peak Table ................................................................................................................. 221 Analysis Channel .................................................................................................. 222 PDA Analysis and Calculations ................................................................................... 222 Chromatograms Extracted from the 3D Data............................................................. 222 Multi-Chromatogram Channels ............................................................................. 222 Working Chromatogram ........................................................................................ 223 Spectra Extracted from the 3D Data .......................................................................... 223 Analysis Spectra ................................................................................................... 223 Working Spectrum................................................................................................. 223 Background Correction ......................................................................................... 223 Spectrum Interpolation .......................................................................................... 224 Spectrum Smoothing ............................................................................................ 224 Spectrum Derivatives ............................................................................................ 224 Upslope and Down slope Spectra......................................................................... 225 Library Search Calculations ....................................................................................... 225 General ................................................................................................................. 225 Pre-Filters .............................................................................................................. 225 Ratio Chromatogram Calculation ............................................................................... 226 Similarity Calculations ................................................................................................ 226 Lambda Max/Min Calculations ................................................................................... 226 Noise Spectrum Calculations ..................................................................................... 227 Peak Purity Calculations ............................................................................................ 227 Background Correction ......................................................................................... 227 Calculating Total Purity ......................................................................................... 227 Three Point Purity ................................................................................................. 228 Spectrum Export ................................................................................................... 228 PDA Data Export ................................................................................................... 229 ChromGate ® Preparative Option .................................................................................. 230 Fraction Collector Configuration ........................................................................... 230 Virtual Fraction Collector Configuration ................................................. 233 Multi Valve Fraction Collector Configuration ......................................... 234 Fraction Collector Setup ....................................................................................... 235 Fraction Collector Instrument Status..................................................................... 247 Fraction Annotations ............................................................................................. 249 Stacked Injection ................................................................................................... 250 SEC Option .................................................................................................................... 257 Overview .................................................................................................................... 257 SEC Calibration..................................................................................................... 257 Applications of SEC .............................................................................................. 258 Using ChromGate ® SEC <strong>Software</strong> ........................................................................ 258 Running an SEC Calibration Standard ................................................................. 259 Single Run Acquisition ............................................................................................... 260 Defining SEC Baseline .......................................................................................... 263 Defining SEC Result Ranges ................................................................................ 263 Define SEC Peaks ................................................................................................ 263 Annotating SEC Chromatograms.......................................................................... 264 SEC Setup ............................................................................................................ 267 SEC Setup Narrow Standard Method ................................................................... 267 SEC Setup Universal Calibration .......................................................................... 270 SEC Setup Broad Range1 Calibration .................................................................. 273 SEC Setup Broad Range 2 Calibration ................................................................. 275
Page 1 and 2: Software ChromGate ® Chromatograph
Page 3: 4 CONTENTS Configuration - Autosamp
Page 7 and 8: 8 Installation Guide ChromGate® 3.
Page 9 and 10: 10 Installation Guide ChromGate® 3
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Page 13 and 14: 14 Short guide ChromGate®, KNAUER
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56 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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170 Knauer Instrument Control Metho
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186 ChromGate® System Suitability
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188 ChromGate® System Suitability
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190 ChromGate® PDA Option Fig. 283
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192 ChromGate® PDA Option calculat
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194 ChromGate® PDA Option (to the
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196 ChromGate® PDA Option PDA View
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216 ChromGate® PDA Option Note tha
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222 PDA Analysis and Calculations c
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224 PDA Analysis and Calculations s
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226 PDA Analysis and Calculations u
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228 PDA Analysis and Calculations 3
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230 ChromGate® Preparative Option
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258 SEC Option Universal Calibratio
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260 SEC Option Fig. 369 Acquisition
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262 SEC Option Amount Values In thi
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264 SEC Option Fig. 373 SEC peak an
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266 SEC Option Fig. 376 Fig. 377 Yo
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268 SEC Option Fig. 379 Enable Anal
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270 SEC Option Export settings Clic
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272 SEC Option All samples analyzed
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274 SEC Option Horizontal Baseline
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276 SEC Option Intrinsic Viscosity
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278 SEC Option Fig. 383 information
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280 SEC Option Fig. 386 Fig. 387 Se
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282 SEC Option single variable sear
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284 Typical Wiring Schemes Typical
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286 Typical Wiring Schemes Fig. 390
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288 Typical Wiring Schemes Fig. 392
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290 Fig. 394 Pump K-1001 / Autosamp
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292 Index Device ID Autosampler 68,
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294 Index R Rack configuration 243
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