ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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ChromGate® Preparative Option 231 Vial Volume [ml] The rack depended value will be displayed automatically. However, you are allowed to overwrite it by self-defined values. If any fraction is larger than the set volume the next free collection position will be used for continued collection. Serial Port Select from the drop-down list the serial port number for the communication port on your PC where the collector is connected. Interface (S 3050 / MultiValve fraction collector / Foxy R1/R2 only) Select the Interface you want to use for communication with the device. RS-232 Select the number for the RS-232 communication port (COM Port) on your PC to which the autosampler is connected. LAN (S 3050, MultiValve fraction collector) To let the software search for your already connected and switchedon device, click on the button to start the search for all connected LAN devices of the currently configured type. The option “Use S/N to identify the instrument” must be enabled. Select the desired device from the shown list. The software will read-out the information as serial number and will fill it automatically into the configuration screen. To search for an instrument, the device must be connected, switched on and must have a valid IP address. As an option, you can enter the IP address of your device, if the option “Use S/N to identify the instrument” is disabled. Please note that in case the device receives the IP address from a DHCP server, e.g. a router, the IP address may change if the device is switched off and switched on. LAN (Foxy FC R1/R2) There is no option for the Foxy fraction collectors to search via LAN or read-out the configuration. If selected, please enter the IP address of the FC. The IP address must match with the IP address in the FC; the Foxy FC R1/R2 do not support LAN with DHCP. The LAN communication is supported in firmware version 1.01.03 and higher. Please note that the touch pad of the Foxy R1/R2 FC will NOT been BLOCKED if the device will be controlled by software. The software cannot recognize inputs via the touch pad. Therefore it is highly recommended, not to use the touch pad under software control. Otherwise the vial position of fractions and other information may not been stored correctly in the „Device Monitor - Show Rack“. The communication port of the fraction collector S 3050 must be select using a switch on the collector’s rear panel. Tubing Parameters Fig. 321 Tubing parameters setup
232 ChromGate® Preparative Option These settings enable someone to consider the time delay for transporting the sample from the flow cell to the collector valve. If the option Use recycling valve is checked, the capillary from the flow cell via the recycling valve to the fractionation valve must be taken into account. If you activate the option Fixed time you can enter this time delay directly. This value will be valid, even if the flow rate is changed! Entering the Capillary Volume directly or calculating it by entering the Capillary Length and Inner Diameter, the delay time will be adapted to the programmed flow rate of the method. Solvent and/or Peak Recycling For an optional solvent and/or peak recycling, for most fraction collectors an additional recycling valve is necessary. As a recycling valve only a Knauer 6-port valve can be used. The Knauer fraction collector 3050 includes a valve for recycling. For a multi valve fraction collector some ports of the fractionation valve can be defined for the recycling. To define a separate recycling valve, check the option Use recycling valve and click on the button. For the separate recycling valve a COM port or the IP address is to define. The settings for the volumetric delay will be displayed without access for changing. The settings are valid as well for the recycling valve as for the fractionation valve. Therefore, the capillary between the recycling valve and the fraction collector should be as short as possible. Only for the Knauer fraction collector 3050 and the multi valve fraction collectors the option Use own ports for recycling will be displayed. If you want to use this option, click into the check box for this option. For the multi valve fraction collector you will find, that the number of available ports for fractionation will be reduced by 2. Additionally the ports numbers for solvent and peak recycling will be shown. It is not possible only to enable one of the recycling options. Fig. 322 Recycling valve setup
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Software ChromGate ® Chromatograph
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4 CONTENTS Configuration - Autosamp
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6 CONTENTS Peak Table .............
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8 Installation Guide ChromGate® 3.
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10 Installation Guide ChromGate® 3
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12 Installation Guide ChromGate® 3
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14 Short guide ChromGate®, KNAUER
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32 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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170 Knauer Instrument Control Metho
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Page 179 and 180: 180 Knauer Instrument Control Metho
Page 185 and 186: 186 ChromGate® System Suitability
Page 187 and 188: 188 ChromGate® System Suitability
Page 189 and 190: 190 ChromGate® PDA Option Fig. 283
Page 191 and 192: 192 ChromGate® PDA Option calculat
Page 193 and 194: 194 ChromGate® PDA Option (to the
Page 195 and 196: 196 ChromGate® PDA Option PDA View
Page 215 and 216: 216 ChromGate® PDA Option Note tha
Page 221 and 222: 222 PDA Analysis and Calculations c
Page 223 and 224: 224 PDA Analysis and Calculations s
Page 225 and 226: 226 PDA Analysis and Calculations u
Page 227 and 228: 228 PDA Analysis and Calculations 3
Page 229: 230 ChromGate® Preparative Option
Page 233 and 234: 234 ChromGate® Preparative Option
Page 257 and 258: 258 SEC Option Universal Calibratio
Page 259 and 260: 260 SEC Option Fig. 369 Acquisition
Page 261 and 262: 262 SEC Option Amount Values In thi
Page 263 and 264: 264 SEC Option Fig. 373 SEC peak an
Page 265 and 266: 266 SEC Option Fig. 376 Fig. 377 Yo
Page 267 and 268: 268 SEC Option Fig. 379 Enable Anal
Page 269 and 270: 270 SEC Option Export settings Clic
Page 271 and 272: 272 SEC Option All samples analyzed
Page 273 and 274: 274 SEC Option Horizontal Baseline
Page 275 and 276: 276 SEC Option Intrinsic Viscosity
Page 277 and 278: 278 SEC Option Fig. 383 information
Page 279 and 280: 280 SEC Option Fig. 386 Fig. 387 Se
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282 SEC Option single variable sear
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284 Typical Wiring Schemes Typical
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286 Typical Wiring Schemes Fig. 390
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288 Typical Wiring Schemes Fig. 392
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290 Fig. 394 Pump K-1001 / Autosamp
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292 Index Device ID Autosampler 68,
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294 Index R Rack configuration 243
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