ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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ChromGate® Preparative Option 235 For use of own ports no further settings are required. Valves number Enter the number of valves which build up the multi valve fraction collector. The number is in practical patterns unlimited. Configure Valve The drop down list offers as many positions as the valve number was entered above. The following settings have to be made for each valve separately. Interface Select the Interface you want to use for communication with the device. RS-232 Select the number for the RS-232 communication port (COM Port) on your PC to which the autosampler is connected. LAN To let the software search for your already connected and switchedon device, click on the button to start the search for all connected LAN devices of the currently configured type. The option “Use S/N to identify the instrument” must be enabled. Select the desired device from the shown list. The software will read-out the information as serial number and will fill it automatically into the configuration screen. To search for an instrument, the device must be connected, switched on and must have a valid IP address. As an option, you can enter the IP address of your device, if the option “Use S/N to identify the instrument” is disabled. Please note that in case the device receives the IP address from a DHCP server, e.g. a router, the IP address may change if the device is switched off and switched on. Valve type The drop down list offers 2-, 6-, 12-, and 16-position valves. Select for each valve the desired type. If you read-out the valve via LAN, the appropriate valve type has been selected automatically. Vial Volume [ml] Enter any desired vial volume. If any fraction is larger than the set volume the next free collection position will be used for continued collection. Vial number The Vial number will be displayed automatically. Fraction Collector Setup In any system you can include only one fraction collector. However, the setup window is independent on the configured fraction collector. Therefore they will be explained together. This window differs in one respect from other setup windows. It is not only important for setting up the fraction collector. You need it also during the runs. However, those aspects will be described later in the chapter instrument status of a (running) control method (page 137).
236 ChromGate® Preparative Option Fig. 328 Fraction collector setup window (upper part) Detection Channel Select from the drop down list of active detector channels that one to be responsible for fractionations. Collector Reset This option must be checked for cumulative collection from repeating runs. Advanced collector settings With a click on the button the Advanced collector settings window will open. Fig. 329 Advanced collector settings Rack Settings If the option Exchange rack if full is enabled, automatically a new, empty rack will be created if the current one is full. A copy of the full rack will be stored; the data from the fractions will not be lost. This allows changing the rack manually during the sequence without starting the sequence again. Is this option disabled, a sequence will stop if no empty vial is left for the next fraction. The Empty vial check tests before the injection, if enough empty vials for the fractions are left. Enter the number of vials needed for one run. The software will check then before the injection, if this number of vials is left. If not, the system will not start the next run. Stacked Injections Restart from first vial of current run If stacked injections are used, check this box if you wants the collector to start for every stacked injection with the same vial as for the previous runs for the fraction collection. This is an option, if you inject the same sample several times and want to collect the fractions of the same substances from every run in the same fraction vials.
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Software ChromGate ® Chromatograph
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4 CONTENTS Configuration - Autosamp
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6 CONTENTS Peak Table .............
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8 Installation Guide ChromGate® 3.
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10 Installation Guide ChromGate® 3
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12 Installation Guide ChromGate® 3
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14 Short guide ChromGate®, KNAUER
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32 Setup and Control of Knauer HPLC
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84 Creating an Instrument Control M
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100 Creating an Instrument Control
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170 Knauer Instrument Control Metho
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Page 183 and 184: 184 Knauer Instrument Control Metho
Page 185 and 186: 186 ChromGate® System Suitability
Page 187 and 188: 188 ChromGate® System Suitability
Page 189 and 190: 190 ChromGate® PDA Option Fig. 283
Page 191 and 192: 192 ChromGate® PDA Option calculat
Page 193 and 194: 194 ChromGate® PDA Option (to the
Page 195 and 196: 196 ChromGate® PDA Option PDA View
Page 215 and 216: 216 ChromGate® PDA Option Note tha
Page 221 and 222: 222 PDA Analysis and Calculations c
Page 223 and 224: 224 PDA Analysis and Calculations s
Page 225 and 226: 226 PDA Analysis and Calculations u
Page 227 and 228: 228 PDA Analysis and Calculations 3
Page 229 and 230: 230 ChromGate® Preparative Option
Page 233: 234 ChromGate® Preparative Option
Page 257 and 258: 258 SEC Option Universal Calibratio
Page 259 and 260: 260 SEC Option Fig. 369 Acquisition
Page 261 and 262: 262 SEC Option Amount Values In thi
Page 263 and 264: 264 SEC Option Fig. 373 SEC peak an
Page 265 and 266: 266 SEC Option Fig. 376 Fig. 377 Yo
Page 267 and 268: 268 SEC Option Fig. 379 Enable Anal
Page 269 and 270: 270 SEC Option Export settings Clic
Page 271 and 272: 272 SEC Option All samples analyzed
Page 273 and 274: 274 SEC Option Horizontal Baseline
Page 275 and 276: 276 SEC Option Intrinsic Viscosity
Page 277 and 278: 278 SEC Option Fig. 383 information
Page 279 and 280: 280 SEC Option Fig. 386 Fig. 387 Se
Page 281 and 282: 282 SEC Option single variable sear
Page 283 and 284: 284 Typical Wiring Schemes Typical
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286 Typical Wiring Schemes Fig. 390
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288 Typical Wiring Schemes Fig. 392
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290 Fig. 394 Pump K-1001 / Autosamp
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292 Index Device ID Autosampler 68,
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294 Index R Rack configuration 243
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ChromeGate 3.3.2 Software Manual - KNAUER Advanced Scientific ...

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