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Abstracts Book - IMRC 2018

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• SF3-P067<br />

SYNTHESIS AND CHARACTERIZATION OF MOLYBDENUM<br />

CARBIDE NANOPARTICLES DOPED WITH NICKEL SUPPORTED IN<br />

CARBON NANOTUBES<br />

Rubén Javier García Pérez 1 , Jonathan Jesús Malpica Maldonado 1 , Jose Aarón Melo Banda 1 ,<br />

David Macias Ferrer 1 , Jose Manuel Dominguez 2<br />

1 Instituto Tecnológico de Ciudad Madero, Centro de Investigación en Petroquímica, Mexico.<br />

2 Instituto Mexicano del Petróleo, ingeniería Molecular, Mexico.<br />

Several studies have demonstrated Ni-Mo2C catalysts exhibits high activity and<br />

selectivity in hydrogen production processes. also, the molybdenum carbide has<br />

shown a catalytic behavior similar as some noble metals, on the other hand,<br />

nickel act as a promoter to increasing selectivity in production of hydrogen. In<br />

this work, Ni-Mo2C nanoparticles were synthesized by carburization of nickel<br />

and molybdenum oxides as precursors and sucrose as carbon source. The<br />

synthesis of Ni-Mo2C was prepared employed the Temperature-programmed<br />

reaction method at 900 °C under hydrogen reducing atmosphere. Also, these<br />

metals were supported in carbon nanotubes (CNTs), The nanotubes are<br />

characterized by having excellent thermal, mechanical and electrical, these<br />

properties made that they have a wide range of applications in engineering. The<br />

samples these materials were characterized by Scanning Transmission Electron<br />

Microscopy (STEM) Energy Dispersive X-ray Spectroscopy. (EDS), Spectroscopy<br />

of photoelectrons emitted by X-ray (XPS), X-Ray Diffraction (XRD) and<br />

Voltammetry.<br />

Keywords: Carbon Nanotubes, Molybdenum Carbide, Hydrogen Production<br />

Presenting authors email: javieruben@gmail.com

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