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Effect of Volume on Synthesis of Silver Nanoparticles from Waste Frying<br />

Palm Oil and Their Catalytic Activities towards Azo Dye<br />

Muhammed Zaim Bin Khariri<br />

Supervisor: Dr. Alyza Azzura binti Abdul Rahman Azmi<br />

Co-Supervisor: Dr. Tuan Nurul Sabiqah binti Tuan Anuar<br />

Bachelor of Science (Analytical and Environmental Chemistry)<br />

School of Marine and Environmental Science<br />

Universiti Malaysia Terengganu<br />

The synthesizing and preparation of silver nanoparticles become widely in research<br />

studies nowadays due to its application in many fields. This study was conducted to<br />

synthesize silver nanoparticles (Ag-NPs) using fatty acids in waste frying palm oil<br />

(WFPO) as reducing agent by using wet chemical method. The parameter that has<br />

been studied in this research is volume of stock solution of WFPO which found to be<br />

directly proportional to yield Ag-NPs. The formation of Ag-NPs was notified by the<br />

presence of yellowish-brown colour of solution and supported by the obtained surface<br />

plasmon resonance (SPR) peak around 415 nm. The synthesized Ag-NPs were further<br />

characterized by UV–Vis spectroscopy, Fourier Transform Infrared (FT-IR)<br />

spectroscopic, X-Ray Powdered Diffraction (XRD), and Scanning Electron Microscopic<br />

(SEM). In addition, the catalytic activities of the Ag-NPs were carried out to determine<br />

the capability of Ag-NPs towards degradation of methyl orange that resulting in<br />

excellent degradation of methyl orange by NaBH4.<br />

1950 | UMT UNDERGRADUATE RESEARCH DAY 2018

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